3,4,6-tri-O-acetyl-2-O-benzoyl-β-D-mannopyranosyl-(1->4)-[2,3,4-tri-O-acetyl-α-L-fucopyranosyl-(1->3)]-2-O-benzoyl-6-O-acetyl-α-D-glucopyranosyl trichloroacetimidate

Base Information

Chemical Name:3,4,6-tri-O-acetyl-2-O-benzoyl-β-D-mannopyranosyl-(1->4)-[2,3,4-tri-O-acetyl-α-L-fucopyranosyl-(1->3)]-2-O-benzoyl-6-O-acetyl-α-D-glucopyranosyl trichloroacetimidate
CAS No.:904319-35-3
Molecular Formula:C₄₈H₅₄Cl₃NO₂₄
Molecular Weight:1135.31
Hs Code.:

3,4,6-tri-O-acetyl-2-O-benzoyl-β-D-mannopyranosyl-(1->4)-[2,3,4-tri-O-acetyl-α-L-fucopyranosyl-(1->3)]-2-O-benzoyl-6-O-acetyl-α-D-glucopyranosyl trichloroacetimidate

Synonyms:3,4,6-tri-O-acetyl-2-O-benzoyl-β-D-mannopyranosyl-(1->4)-[2,3,4-tri-O-acetyl-α-L-fucopyranosyl-(1->3)]-2-O-benzoyl-6-O-acetyl-α-D-glucopyranosyl trichloroacetimidate

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Chemical Property of 3,4,6-tri-O-acetyl-2-O-benzoyl-β-D-mannopyranosyl-(1->4)-[2,3,4-tri-O-acetyl-α-L-fucopyranosyl-(1->3)]-2-O-benzoyl-6-O-acetyl-α-D-glucopyranosyl trichloroacetimidate

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Technology Process of 3,4,6-tri-O-acetyl-2-O-benzoyl-β-D-mannopyranosyl-(1->4)-[2,3,4-tri-O-acetyl-α-L-fucopyranosyl-(1->3)]-2-O-benzoyl-6-O-acetyl-α-D-glucopyranosyl trichloroacetimidate

There total 1 articles about 3,4,6-tri-O-acetyl-2-O-benzoyl-β-D-mannopyranosyl-(1->4)-[2,3,4-tri-O-acetyl-α-L-fucopyranosyl-(1->3)]-2-O-benzoyl-6-O-acetyl-α-D-glucopyranosyl trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 904319-34-2
2-(trimethylsilyl)ethyl 3,4,6-tri-O-acetyl-2-O-benzoyl-β-D-mannopyranosyl-(1->4)-[2,3,4-tri-O-acetyl-α-L-fucopyranosyl-(1->3)]-2-O-benzoyl-6-O-acetyl-β-D-glucopyranoside

: 545-06-2
trichloroacetonitrile

: 904319-35-3
3,4,6-tri-O-acetyl-2-O-benzoyl-β-D-mannopyranosyl-(1->4)-[2,3,4-tri-O-acetyl-α-L-fucopyranosyl-(1->3)]-2-O-benzoyl-6-O-acetyl-α-D-glucopyranosyl trichloroacetimidate

Guidance literature:: 2-(trimethylsilyl)ethyl 3,4,6-tri-O-acetyl-2-O-benzoyl-β-D-mannopyranosyl-(1->4)-[2,3,4-tri-O-acetyl-α-L-fucopyranosyl-(1->3)]-2-O-benzoyl-6-O-acetyl-β-D-glucopyranoside; With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; for 2.5h;

trichloroacetonitrile; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In dichloromethane; at 0 ℃; for 2h;
DOI:10.1016/j.carres.2006.04.019

Reference yield: 35.0%

: 904319-35-3
3,4,6-tri-O-acetyl-2-O-benzoyl-β-D-mannopyranosyl-(1->4)-[2,3,4-tri-O-acetyl-α-L-fucopyranosyl-(1->3)]-2-O-benzoyl-6-O-acetyl-α-D-glucopyranosyl trichloroacetimidate

: 4201-55-2
(2S,3R,4E)-3-benzoyl-2-(hexadecanamido)-4-octadecene-1,3-diol

: 3,4,6-tri-O-acetyl-2-O-benzoyl-β-D-mannopyranosyl-(1->4)-[2,3,4-tri-O-acetyl-α-L-fucopyranosyl-(1->3)]-2-O-benzoyl-6-O-acetyl-β-D-glucopyranosyl-(1->1)-(2S,3R,4E)-3-O-benzoyl-2-hexadecanamido-4-octadecene-1,3-diol

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; In dichloromethane; at 0 ℃;
DOI:10.1016/j.carres.2006.04.019

Reference yield:

: 904319-35-3
3,4,6-tri-O-acetyl-2-O-benzoyl-β-D-mannopyranosyl-(1->4)-[2,3,4-tri-O-acetyl-α-L-fucopyranosyl-(1->3)]-2-O-benzoyl-6-O-acetyl-α-D-glucopyranosyl trichloroacetimidate

: 904319-39-7
C₆₄H₈₃Cl₃N₂O₂₉

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / AW₃₀₀ molecular sieves; TMSOTf / CH₂Cl₂ / 4 h / 0 °C

2: 100 percent / HOAc; zinc powder / 16 h / 20 °C

3: 66 percent / Et₃N; DEPC / dimethylformamide / 16 h / 20 °C

With molecular sieve; trimethylsilyl trifluoromethanesulfonate; acetic acid; triethylamine; diethyl dicarbonate; zinc; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/j.carres.2006.04.019