Technology Process of C45H78N2O12
There total 8 articles about C45H78N2O12 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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Multi-step reaction with 6 steps
1.1: ammonium hydroxide / methanol / 6 h / 20 °C
2.1: sodium tris(acetoxy)borohydride / chloroform / 4 h / 20 °C
3.1: sodium tris(acetoxy)borohydride / chloroform; water / 1 h / 20 °C
4.1: water; lithium hydroxide monohydrate / tetrahydrofuran; ethanol / 6 h / 20 °C
5.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / tetrahydrofuran / 2 h / 20 °C
5.2: 0.5 h / Reflux
6.1: pyridine hydrogenfluoride / tetrahydrofuran / 18 h / 20 °C
With
ammonium hydroxide; lithium hydroxide monohydrate; 2,4,6-trichlorobenzoyl chloride; water; sodium tris(acetoxy)borohydride; pyridine hydrogenfluoride; triethylamine;
In
tetrahydrofuran; methanol; ethanol; chloroform; water;
DOI:10.1016/j.bmc.2012.08.007
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium tris(acetoxy)borohydride / chloroform; water / 1 h / 20 °C
2.1: water; lithium hydroxide monohydrate / tetrahydrofuran; ethanol / 6 h / 20 °C
3.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / tetrahydrofuran / 2 h / 20 °C
3.2: 0.5 h / Reflux
4.1: pyridine hydrogenfluoride / tetrahydrofuran / 18 h / 20 °C
With
lithium hydroxide monohydrate; 2,4,6-trichlorobenzoyl chloride; water; sodium tris(acetoxy)borohydride; pyridine hydrogenfluoride; triethylamine;
In
tetrahydrofuran; ethanol; chloroform; water;
DOI:10.1016/j.bmc.2012.08.007