1ξ-oxo-6β-(2-phenyl-acetylamino)-1λ⁴-penicillanic acid 4-nitro-benzyl ester

Base Information

Chemical Name:1ξ-oxo-6β-(2-phenyl-acetylamino)-1λ⁴-penicillanic acid 4-nitro-benzyl ester
CAS No.:29124-80-9
Molecular Formula:C₂₃H₂₃N₃O₇S
Molecular Weight:485.518
Hs Code.:

1ξ-oxo-6β-(2-phenyl-acetylamino)-1λ<sup>4</sup>-penicillanic acid 4-nitro-benzyl ester

Synonyms:1ξ-oxo-6β-(2-phenyl-acetylamino)-1λ⁴-penicillanic acid 4-nitro-benzyl ester

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Chemical Property of 1ξ-oxo-6β-(2-phenyl-acetylamino)-1λ⁴-penicillanic acid 4-nitro-benzyl ester

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Technology Process of 1ξ-oxo-6β-(2-phenyl-acetylamino)-1λ⁴-penicillanic acid 4-nitro-benzyl ester

There total 3 articles about 1ξ-oxo-6β-(2-phenyl-acetylamino)-1λ⁴-penicillanic acid 4-nitro-benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.4%

: 27487-21-4
p-nitrobenzyl benzylpenicillinate

: 29124-80-9
1ξ-oxo-6β-(2-phenyl-acetylamino)-1λ⁴-penicillanic acid 4-nitro-benzyl ester

Guidance literature:: With peracetic acid; at 0 - 20 ℃; for 2h; Temperature; Large scale;

Reference yield:

: 100-11-8
1-bromomethyl-4-nitro-benzene

: 29124-80-9
1ξ-oxo-6β-(2-phenyl-acetylamino)-1λ⁴-penicillanic acid 4-nitro-benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: N,N-dimethyl-formamide / 2 h / 42 - 45 °C / Large scale

1.2: 2 h / 0 - 5 °C / Large scale

2.1: sodium sulfite / water / Large scale

2.2: 0.5 h / Large scale

With sodium sulfite; In water; N,N-dimethyl-formamide;

Reference yield:

: 113-98-4
Penicillin G potassium

: 29124-80-9
1ξ-oxo-6β-(2-phenyl-acetylamino)-1λ⁴-penicillanic acid 4-nitro-benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: N,N-dimethyl-formamide / 2 h / 42 - 45 °C / Large scale

1.2: 2 h / 0 - 5 °C / Large scale

2.1: sodium sulfite / water / Large scale

2.2: 0.5 h / Large scale

With sodium sulfite; In water; N,N-dimethyl-formamide;