allyl (3,6-di-O-acetyl-2,4-di-O-benzoyl-β-D-glucopyranosyl)-(1->3)-4,6-O-benzylidene-2-O-benzoyl-β-D-galactopyranoside

Base Information

• Chemical Name: allyl (3,6-di-O-acetyl-2,4-di-O-benzoyl-β-D-glucopyranosyl)-(1->3)-4,6-O-benzylidene-2-O-benzoyl-β-D-galactopyranoside
• CAS No.: 1082471-44-0
• Molecular Formula: C₄₇H₄₆O₁₆
• Molecular Weight: 866.873

Synonyms:allyl (3,6-di-O-acetyl-2,4-di-O-benzoyl-β-D-glucopyranosyl)-(1->3)-4,6-O-benzylidene-2-O-benzoyl-β-D-galactopyranoside

Chemical Property of allyl (3,6-di-O-acetyl-2,4-di-O-benzoyl-β-D-glucopyranosyl)-(1->3)-4,6-O-benzylidene-2-O-benzoyl-β-D-galactopyranoside

Chemical Property:

Purity/Quality:

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Technology Process of allyl (3,6-di-O-acetyl-2,4-di-O-benzoyl-β-D-glucopyranosyl)-(1->3)-4,6-O-benzylidene-2-O-benzoyl-β-D-galactopyranoside

There total 1 articles about allyl (3,6-di-O-acetyl-2,4-di-O-benzoyl-β-D-glucopyranosyl)-(1->3)-4,6-O-benzylidene-2-O-benzoyl-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

3,6-di-O-acetyl-2,4-di-O-benzoyl-α-D-glucopyranosyl trichloroacetimidate + allyl 2-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranoside (155835-94-2) → allyl (3,6-di-O-acetyl-2,4-di-O-benzoyl-β-D-glucopyranosyl)-(1->3)-4,6-O-benzylidene-2-O-benzoyl-β-D-galactopyranoside (1082471-44-0)

Guidance literature:

With 3 A molecular sieve; boron trifluoride diethyl etherate; In toluene; at 4 - 10 ℃; for 50.5h;

DOI:10.1007/s11172-007-0258-y

Reference yield: 98.0%

allyl (3,6-di-O-acetyl-2,4-di-O-benzoyl-β-D-glucopyranosyl)-(1->3)-4,6-O-benzylidene-2-O-benzoyl-β-D-galactopyranoside (1082471-44-0) → allyl (3,6-di-O-acetyl-2,4-di-O-benzoyl-β-D-glucopyranosyl)-(1->3)-2-O-benzoyl-β-D-galactopyranoside

Guidance literature:

With pyridinium p-toluenesulfonate; In water; acetonitrile; at 80 ℃; for 36h;

DOI:10.1007/s11172-007-0258-y

upstream raw materials:

allyl 2-O-benzoyl-4,6-O-benzylidene-β-D-galactopyranoside

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