Technology Process of 3,6-di(2-nitrophenyl)-2,7-dioctyloxynaphthalene
There total 4 articles about 3,6-di(2-nitrophenyl)-2,7-dioctyloxynaphthalene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrakis(triphenylphosphine) palladium(0); sodium carbonate;
In
water; toluene;
at 20 ℃;
Reflux;
Inert atmosphere;
DOI:10.1021/ol101076m
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: bromine; tin / acetic acid / Inert atmosphere; Heating
2.1: potassium carbonate / acetonitrile / Inert atmosphere; Heating
3.1: n-butyllithium / diethyl ether / Inert atmosphere
3.2: Inert atmosphere
4.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / toluene / Inert atmosphere; Heating
With
tin; tetrakis(triphenylphosphine) palladium(0); n-butyllithium; bromine; sodium carbonate; potassium carbonate;
In
diethyl ether; acetic acid; toluene; acetonitrile;
4.1: |Suzuki-Miyaura Coupling;
DOI:10.1039/c2tc00363e
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate / acetonitrile / Inert atmosphere; Heating
2.1: n-butyllithium / diethyl ether / Inert atmosphere
2.2: Inert atmosphere
3.1: tetrakis(triphenylphosphine) palladium(0); sodium carbonate / toluene / Inert atmosphere; Heating
With
tetrakis(triphenylphosphine) palladium(0); n-butyllithium; sodium carbonate; potassium carbonate;
In
diethyl ether; toluene; acetonitrile;
3.1: |Suzuki-Miyaura Coupling;
DOI:10.1039/c2tc00363e
