(S,S)-N-(2-amino-1,2-diphenyl-ethyl)-2,3,4,5,6-pentamethyl-benzene sulfonamide

Base Information

• Chemical Name: (S,S)-N-(2-amino-1,2-diphenyl-ethyl)-2,3,4,5,6-pentamethyl-benzene sulfonamide
• CAS No.: 1175672-03-3
• Molecular Formula: C₂₅H₃₀N₂O₂S
• Molecular Weight: 422.591

Synonyms:(S,S)-N-(2-amino-1,2-diphenyl-ethyl)-2,3,4,5,6-pentamethyl-benzene sulfonamide

Chemical Property of (S,S)-N-(2-amino-1,2-diphenyl-ethyl)-2,3,4,5,6-pentamethyl-benzene sulfonamide

Chemical Property:

Purity/Quality:

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Technology Process of (S,S)-N-(2-amino-1,2-diphenyl-ethyl)-2,3,4,5,6-pentamethyl-benzene sulfonamide

There total 1 articles about (S,S)-N-(2-amino-1,2-diphenyl-ethyl)-2,3,4,5,6-pentamethyl-benzene sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

(S,S)-1,2-diphenyl-1,2-diaminoethane (29841-69-8) + 2,3,4,5,6-pentamethylbenzenesulfonyl chloride (52499-94-2) → (S,S)-N-(2-amino-1,2-diphenyl-ethyl)-2,3,4,5,6-pentamethyl-benzene sulfonamide (1175672-03-3)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃;

DOI:10.1016/j.tet.2009.05.012

Reference yield:

(S,S)-N-(2-amino-1,2-diphenyl-ethyl)-2,3,4,5,6-pentamethyl-benzene sulfonamide (1175672-03-3) + propionaldehyde (123-38-6) → C28H34N2O2S

Guidance literature:

With acetic acid; In methanol; for 3h; Molecular sieve;

DOI:10.1016/j.tet.2009.05.012

Reference yield:

bis[dichloro(pentamethylcyclopentadienyl)iridium(III)] (12354-84-6,12354-85-7) + (S,S)-N-(2-amino-1,2-diphenyl-ethyl)-2,3,4,5,6-pentamethyl-benzene sulfonamide (1175672-03-3) → (C5(CH3)5)Ir(NHCH(C6H5)CH(C6H5)NSO2C6(CH3)5)

Guidance literature:

With potassium hydroxide; In dichloromethane; water; for 0.5h; Inert atmosphere;

DOI:10.1002/anie.201307789

upstream raw materials:

(S,S)-1,2-diphenyl-1,2-diaminoethane

2,3,4,5,6-pentamethylbenzenesulfonyl chloride

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