Technology Process of C45H65O11N(13)C4
There total 8 articles about C45H65O11N(13)C4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
1,8-diazabicyclo[5.4.0]undec-7-ene;
In
acetonitrile;
at 20 ℃;
DOI:10.1002/jlcr.1240
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 51 percent / H2 / PtO2 / ethyl acetate / 20 °C
2: 66 percent / PhNMe2 / CH2Cl2 / 20 °C
3: 73 percent / DBU / acetonitrile / 20 °C
With
hydrogen; N,N-dimethyl-aniline; 1,8-diazabicyclo[5.4.0]undec-7-ene;
platinum(IV) oxide;
In
dichloromethane; ethyl acetate; acetonitrile;
3: Wittig-Horner-Emmons reaction;
DOI:10.1002/jlcr.1240
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 89 percent / DMAP / acetonitrile / 20 °C
2: 51 percent / H2 / PtO2 / ethyl acetate / 20 °C
3: 66 percent / PhNMe2 / CH2Cl2 / 20 °C
4: 73 percent / DBU / acetonitrile / 20 °C
With
dmap; hydrogen; N,N-dimethyl-aniline; 1,8-diazabicyclo[5.4.0]undec-7-ene;
platinum(IV) oxide;
In
dichloromethane; ethyl acetate; acetonitrile;
4: Wittig-Horner-Emmons reaction;
DOI:10.1002/jlcr.1240