N-({4-[3-(aminooxy)propyl]phenyl}methyl)prop-2-enyloxycarboxamide hydrochloric acid salt

Base Information

Chemical Name:N-({4-[3-(aminooxy)propyl]phenyl}methyl)prop-2-enyloxycarboxamide hydrochloric acid salt
CAS No.:1173158-33-2
Molecular Formula:C₁₄H₂₀N₂O₃*ClH
Molecular Weight:300.785
Hs Code.:

Synonyms:N-({4-[3-(aminooxy)propyl]phenyl}methyl)prop-2-enyloxycarboxamide hydrochloric acid salt

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Chemical Property of N-({4-[3-(aminooxy)propyl]phenyl}methyl)prop-2-enyloxycarboxamide hydrochloric acid salt

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Technology Process of N-({4-[3-(aminooxy)propyl]phenyl}methyl)prop-2-enyloxycarboxamide hydrochloric acid salt

There total 5 articles about N-({4-[3-(aminooxy)propyl]phenyl}methyl)prop-2-enyloxycarboxamide hydrochloric acid salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1173158-36-5
C₂₂H₂₂N₂O₅

: 1173158-33-2
N-({4-[3-(aminooxy)propyl]phenyl}methyl)prop-2-enyloxycarboxamide hydrochloric acid salt

Guidance literature:: C₂₂H₂₂N₂O₅; With hydrazine; In methanol; chloroform; at 22 ℃; for 0.5h;

With hydrogenchloride; In 1,4-dioxane; diethyl ether;

Reference yield:

: 16642-94-7,18664-39-6
(E)-4-cyanocinnamic acid

: 1173158-33-2
N-({4-[3-(aminooxy)propyl]phenyl}methyl)prop-2-enyloxycarboxamide hydrochloric acid salt

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogen; ammonia / Raney Ni / water; methanol / 22 °C / 2585.81 Torr

2.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1.67 h / 22 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 3.33 h / 0 - 22 °C

3.2: 0.5 h

4.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 0 - 22 °C

5.1: hydrazine / chloroform; methanol / 0.5 h / 22 °C

With lithium aluminium tetrahydride; ammonia; hydrogen; N-ethyl-N,N-diisopropylamine; triphenylphosphine; hydrazine; diethylazodicarboxylate; Raney Ni; In tetrahydrofuran; methanol; chloroform; water;

Reference yield:

: 55197-36-9
3-(4-aminomethyl-phenyl)-propionic acid

: 1173158-33-2
N-({4-[3-(aminooxy)propyl]phenyl}methyl)prop-2-enyloxycarboxamide hydrochloric acid salt

Guidance literature:: Multi-step reaction with 4 steps

1.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1.67 h / 22 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 3.33 h / 0 - 22 °C

2.2: 0.5 h

3.1: triphenylphosphine; diethylazodicarboxylate / tetrahydrofuran / 0 - 22 °C

4.1: hydrazine / chloroform; methanol / 0.5 h / 22 °C

With lithium aluminium tetrahydride; N-ethyl-N,N-diisopropylamine; triphenylphosphine; hydrazine; diethylazodicarboxylate; In tetrahydrofuran; methanol; chloroform;