C₃₁H₃₇F

Base Information

Chemical Name:C₃₁H₃₇F
CAS No.:1402734-14-8
Molecular Formula:C₃₁H₃₇F
Molecular Weight:428.633
Hs Code.:

Synonyms:C₃₁H₃₇F

Suppliers and Price of C₃₁H₃₇F

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Chemical Property of C₃₁H₃₇F

Chemical Property:

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Technology Process of C₃₁H₃₇F

There total 7 articles about C₃₁H₃₇F which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1402734-18-2
C₃₁H₃₅F

: 1402734-14-8
C₃₁H₃₇F

Guidance literature:: With hydrogen; palladium 10% on activated carbon; In methanol; toluene; for 8h;

Reference yield:

: 958654-11-0
3-fluoro-4-iodo-4'-propylbiphenyl

: 1402734-14-8
C₃₁H₃₇F

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾; Aliquat 336 / toluene; water / 12 h / 85 °C

2.1: hydrogenchloride; sodium nitrite / water; tetrahydrofuran / 0.17 h / Cooling with ice

2.2: 1 h / 0 - 20 °C

3.1: n-butyllithium / tetrahydrofuran / 0.5 h / -78 °C

3.2: 20 °C

3.3: 2 h / 120 °C

4.1: hydrogen / palladium 10% on activated carbon / toluene; methanol / 8 h

With hydrogenchloride; n-butyllithium; hydrogen; potassium carbonate; sodium nitrite; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; Aliquat 336; In tetrahydrofuran; methanol; water; toluene;

Reference yield:

: 1179141-54-8
C₁₅H₁₆FN

: 1402734-14-8
C₃₁H₃₇F

Guidance literature:: Multi-step reaction with 5 steps

1.1: hydrogenchloride; sodium nitrite / water; tetrahydrofuran / 0.17 h / Cooling with ice

1.2: 1 h / 0 - 20 °C

2.1: potassium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾; Aliquat 336 / toluene; water / 12 h / 85 °C

3.1: hydrogenchloride; sodium nitrite / water; tetrahydrofuran / 0.17 h / Cooling with ice

3.2: 1 h / 0 - 20 °C

4.1: n-butyllithium / tetrahydrofuran / 0.5 h / -78 °C

4.2: 20 °C

4.3: 2 h / 120 °C

5.1: hydrogen / palladium 10% on activated carbon / toluene; methanol / 8 h

With hydrogenchloride; n-butyllithium; hydrogen; potassium carbonate; sodium nitrite; tetrakis(triphenylphosphine) palladium⁽⁰⁾; palladium 10% on activated carbon; Aliquat 336; In tetrahydrofuran; methanol; water; toluene;