Technology Process of C27H37BO3Si
There total 5 articles about C27H37BO3Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
pyridine;
In
toluene;
at 20 ℃;
for 12h;
Inert atmosphere;
Glovebox;
DOI:10.1021/ja3070717
- Guidance literature:
-
Multi-step reaction with 3 steps
1: tetrakis(triphenylphosphine) palladium(0); copper(l) iodide; diethylamine / 12 h / 20 °C / Inert atmosphere; Cooling with ice
2: palladium(II) acetylacetonate; triethylphosphine; diisobutylaluminium hydride / toluene / 24 h / 20 °C / Inert atmosphere; Glovebox
3: pyridine / toluene / 12 h / 20 °C / Inert atmosphere; Glovebox
With
pyridine; palladium(II) acetylacetonate; copper(l) iodide; tetrakis(triphenylphosphine) palladium(0); diisobutylaluminium hydride; diethylamine; triethylphosphine;
In
toluene;
DOI:10.1021/ja3070717
- Guidance literature:
-
Multi-step reaction with 2 steps
1: palladium(II) acetylacetonate; triethylphosphine; diisobutylaluminium hydride / toluene / 24 h / 20 °C / Inert atmosphere; Glovebox
2: pyridine / toluene / 12 h / 20 °C / Inert atmosphere; Glovebox
With
pyridine; palladium(II) acetylacetonate; diisobutylaluminium hydride; triethylphosphine;
In
toluene;
DOI:10.1021/ja3070717