C₂₀H₃₀INO₃

Base Information

Chemical Name:C₂₀H₃₀INO₃
CAS No.:1391732-31-2
Molecular Formula:C₂₀H₃₀INO₃
Molecular Weight:459.368
Hs Code.:

C<sub>20</sub>H<sub>30</sub>INO<sub>3</sub>

Synonyms:C₂₀H₃₀INO₃

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Chemical Property of C₂₀H₃₀INO₃

Chemical Property:

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Technology Process of C₂₀H₃₀INO₃

There total 5 articles about C₂₀H₃₀INO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 596104-60-8
(2-nonyl-[1,3]dioxolan-2-yl)-acetic acid

: 626-01-7
3-Iodoaniline

: 1391732-31-2
C₂₀H₃₀INO₃

Guidance literature:: (2-nonyl-[1,3]dioxolan-2-yl)-acetic acid; With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 0.333333h; Inert atmosphere;

3-Iodoaniline; In dichloromethane; at 20 ℃; for 18h;
DOI:10.1039/c2ob25198a

Reference yield:

: 112-13-0
n-decanoyl chloride

: 1391732-31-2
C₂₀H₃₀INO₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: pyridine / dichloromethane / 0 - 20 °C / Inert atmosphere

2.1: Reflux; Inert atmosphere

3.1: toluene-4-sulfonic acid; trimethyl orthoformate / 20 °C / Inert atmosphere

4.1: water; sodium hydroxide / 20 °C / Inert atmosphere

5.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 0.33 h / 20 °C / Inert atmosphere

5.2: 18 h / 20 °C

With pyridine; dmap; water; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; sodium hydroxide; trimethyl orthoformate; In dichloromethane;
DOI:10.1039/c2ob25198a

Reference yield:

: 429675-23-0
5-(1-hydroxydecylidene)-2,2-dimethyl-1,3-dioxane-4,6-dione

: 1391732-31-2
C₂₀H₃₀INO₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: Reflux; Inert atmosphere

2.1: toluene-4-sulfonic acid; trimethyl orthoformate / 20 °C / Inert atmosphere

3.1: water; sodium hydroxide / 20 °C / Inert atmosphere

4.1: dmap; dicyclohexyl-carbodiimide / dichloromethane / 0.33 h / 20 °C / Inert atmosphere

4.2: 18 h / 20 °C

With dmap; water; toluene-4-sulfonic acid; dicyclohexyl-carbodiimide; sodium hydroxide; trimethyl orthoformate; In dichloromethane;
DOI:10.1039/c2ob25198a