2-<2-<(1,1-dimethylethyl)dimethylsilyl>ethynyl>-3,4,5-trimethoxybenzenemethanol TMS ether

Base Information

• Chemical Name: 2-<2-<(1,1-dimethylethyl)dimethylsilyl>ethynyl>-3,4,5-trimethoxybenzenemethanol TMS ether
• CAS No.: 117370-35-1
• Molecular Formula: C₂₁H₃₆O₄Si₂
• Molecular Weight: 408.685
• Mol file: 117370-35-1.mol

Synonyms:2-<2-<(1,1-dimethylethyl)dimethylsilyl>ethynyl>-3,4,5-trimethoxybenzenemethanol TMS ether

Chemical Property of 2-<2-<(1,1-dimethylethyl)dimethylsilyl>ethynyl>-3,4,5-trimethoxybenzenemethanol TMS ether

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of 2-<2-<(1,1-dimethylethyl)dimethylsilyl>ethynyl>-3,4,5-trimethoxybenzenemethanol TMS ether

There total 1 articles about 2-<2-<(1,1-dimethylethyl)dimethylsilyl>ethynyl>-3,4,5-trimethoxybenzenemethanol TMS ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

(tert-butyldimethylsilyl)acetylene (86318-61-8) + (2-Iodo-3,4,5-trimethoxy-benzyloxy)-trimethyl-silane (117370-30-6) → 2-<2-<(1,1-dimethylethyl)dimethylsilyl>ethynyl>-3,4,5-trimethoxybenzenemethanol TMS ether (117370-35-1)

Guidance literature:

With palladium diacetate; triphenylphosphine; In triethylamine; for 4h; Heating;

DOI:10.1021/jo00262a053

upstream raw materials:

(tert-butyldimethylsilyl)acetylene

(2-Iodo-3,4,5-trimethoxy-benzyloxy)-trimethyl-silane