4-[S-(3-bromophenyl)-N-(3-{N,N-bismethanesulfonylamino}benzene-sulfonyl)sulfoximino]-5-methylsulfanyl-thiophene-2-carboxamidine trifluoroacetate

Base Information

Chemical Name:4-[S-(3-bromophenyl)-N-(3-{N,N-bismethanesulfonylamino}benzene-sulfonyl)sulfoximino]-5-methylsulfanyl-thiophene-2-carboxamidine trifluoroacetate
CAS No.:911029-10-2
Molecular Formula:C₂HF₃O₂*C₂₀H₂₁BrN₄O₇S₆
Molecular Weight:815.733
Hs Code.:

4-[S-(3-bromophenyl)-N-(3-{N,N-bismethanesulfonylamino}benzene-sulfonyl)sulfoximino]-5-methylsulfanyl-thiophene-2-carboxamidine trifluoroacetate

Synonyms:4-[S-(3-bromophenyl)-N-(3-{N,N-bismethanesulfonylamino}benzene-sulfonyl)sulfoximino]-5-methylsulfanyl-thiophene-2-carboxamidine trifluoroacetate

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Chemical Property of 4-[S-(3-bromophenyl)-N-(3-{N,N-bismethanesulfonylamino}benzene-sulfonyl)sulfoximino]-5-methylsulfanyl-thiophene-2-carboxamidine trifluoroacetate

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Technology Process of 4-[S-(3-bromophenyl)-N-(3-{N,N-bismethanesulfonylamino}benzene-sulfonyl)sulfoximino]-5-methylsulfanyl-thiophene-2-carboxamidine trifluoroacetate

There total 23 articles about 4-[S-(3-bromophenyl)-N-(3-{N,N-bismethanesulfonylamino}benzene-sulfonyl)sulfoximino]-5-methylsulfanyl-thiophene-2-carboxamidine trifluoroacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₅H₂₉BrN₄O₉S₆

: 76-05-1
trifluoroacetic acid

: 911029-10-2
4-[S-(3-bromophenyl)-N-(3-{N,N-bismethanesulfonylamino}benzene-sulfonyl)sulfoximino]-5-methylsulfanyl-thiophene-2-carboxamidine trifluoroacetate

Guidance literature:: In dichloromethane; at 20 ℃; for 1.5h;

Reference yield:

: 911030-33-6
methyl 3-bromobenzenesulfinate

: 911029-10-2
4-[S-(3-bromophenyl)-N-(3-{N,N-bismethanesulfonylamino}benzene-sulfonyl)sulfoximino]-5-methylsulfanyl-thiophene-2-carboxamidine trifluoroacetate

Guidance literature:: Multi-step reaction with 8 steps

1.1: isopropylmagnesium chloride / tetrahydrofuran / 1.5 h / -78 °C

1.2: -78 - 20 °C

2.1: copper(II) bis(trifluoromethanesulfonate) / acetonitrile / 1 h / 20 °C

3.1: tetrahydrofuran; methanol / 1.5 h / -78 - 20 °C

4.1: ammonia; ammonium formate / tetrahydrofuran; methanol / 16 h / 40 °C

5.1: N-ethyl-N,N-diisopropylamine / 1,4-dioxane; methanol / 4 h / 20 °C

6.1: iron; ammonium chloride / methanol; water / 1 h / 80 °C / Heating / reflux

7.1: triethylamine / dichloromethane / 1.5 h / 20 °C

8.1: dichloromethane / 1.5 h / 20 °C

With ammonia; isopropylmagnesium chloride; ammonium formate; iron; ammonium chloride; triethylamine; N-ethyl-N,N-diisopropylamine; copper(II) bis(trifluoromethanesulfonate); In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; acetonitrile;

Reference yield:

: 6320-01-0
3-Bromothiophenol

: 911029-10-2
4-[S-(3-bromophenyl)-N-(3-{N,N-bismethanesulfonylamino}benzene-sulfonyl)sulfoximino]-5-methylsulfanyl-thiophene-2-carboxamidine trifluoroacetate

Guidance literature:: Multi-step reaction with 10 steps

1.1: pyridinium chlorochromate / dichloromethane / 1 h / 0 - 20 °C

2.1: bromine; sodium carbonate / 20 °C

3.1: isopropylmagnesium chloride / tetrahydrofuran / 1.5 h / -78 °C

3.2: -78 - 20 °C

4.1: copper(II) bis(trifluoromethanesulfonate) / acetonitrile / 1 h / 20 °C

5.1: tetrahydrofuran; methanol / 1.5 h / -78 - 20 °C

6.1: ammonia; ammonium formate / tetrahydrofuran; methanol / 16 h / 40 °C

7.1: N-ethyl-N,N-diisopropylamine / 1,4-dioxane; methanol / 4 h / 20 °C

8.1: iron; ammonium chloride / methanol; water / 1 h / 80 °C / Heating / reflux

9.1: triethylamine / dichloromethane / 1.5 h / 20 °C

10.1: dichloromethane / 1.5 h / 20 °C

With ammonia; bromine; isopropylmagnesium chloride; ammonium formate; iron; sodium carbonate; ammonium chloride; triethylamine; N-ethyl-N,N-diisopropylamine; pyridinium chlorochromate; copper(II) bis(trifluoromethanesulfonate); In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; acetonitrile;