C₃₂H₅₄O₄Si₂

Base Information

Chemical Name:C₃₂H₅₄O₄Si₂
CAS No.:1360872-82-7
Molecular Formula:C₃₂H₅₄O₄Si₂
Molecular Weight:558.949
Hs Code.:

C<sub>32</sub>H<sub>54</sub>O<sub>4</sub>Si<sub>2</sub>

Synonyms:C₃₂H₅₄O₄Si₂

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Chemical Property of C₃₂H₅₄O₄Si₂

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Technology Process of C₃₂H₅₄O₄Si₂

There total 8 articles about C₃₂H₅₄O₄Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1360872-96-3
C₄₀H₆₂O₅Si₂

: 1360872-82-7
C₃₂H₅₄O₄Si₂

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; at 0 - 20 ℃; pH=7; aq. phosphate buffer;
DOI:10.1002/chem.201101437

Reference yield:

: 1360872-91-8
C₃₀H₃₈O₄Si

: 1360872-82-7
C₃₂H₅₄O₄Si₂

Guidance literature:: Multi-step reaction with 6 steps

1.1: copper(l) iodide / tetrahydrofuran; diethyl ether / 0.17 h / -40 °C

1.2: 0.75 h / -40 °C

2.1: Dess-Martin periodane / dichloromethane / 0 - 20 °C

3.1: tetrahydrofuran; diethyl ether / 0.5 h / -78 °C

4.1: 2,6-dimethylpyridine / dichloromethane / 4.5 h / 20 °C

5.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 3 h / 20 °C

5.2: 1 h / 20 °C

6.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 0 - 20 °C / pH 7 / aq. phosphate buffer

With 2,6-dimethylpyridine; copper(l) iodide; Dess-Martin periodane; 9-bora-bicyclo[3.3.1]nonane; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1002/chem.201101437

Reference yield:

: 1360872-90-7
C₃₀H₄₀O₅Si

: 1360872-82-7
C₃₂H₅₄O₄Si₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C

1.2: 3 h / -78 - 20 °C

2.1: copper(l) iodide / tetrahydrofuran; diethyl ether / 0.17 h / -40 °C

2.2: 0.75 h / -40 °C

3.1: Dess-Martin periodane / dichloromethane / 0 - 20 °C

4.1: tetrahydrofuran; diethyl ether / 0.5 h / -78 °C

5.1: 2,6-dimethylpyridine / dichloromethane / 4.5 h / 20 °C

6.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 3 h / 20 °C

6.2: 1 h / 20 °C

7.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 0 - 20 °C / pH 7 / aq. phosphate buffer

With 2,6-dimethylpyridine; copper(l) iodide; sodium hydride; Dess-Martin periodane; 9-bora-bicyclo[3.3.1]nonane; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; diethyl ether; dichloromethane; mineral oil;
DOI:10.1002/chem.201101437