(2-(diphenylphosphanyl)benzaldehyde benzoylhydrazonato)PdMe

Base Information

Chemical Name:(2-(diphenylphosphanyl)benzaldehyde benzoylhydrazonato)PdMe
CAS No.:422313-59-5
Molecular Formula:C₂₇H₂₃N₂OPPd
Molecular Weight:528.886
Hs Code.:

Synonyms:(2-(diphenylphosphanyl)benzaldehyde benzoylhydrazonato)PdMe

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Chemical Property of (2-(diphenylphosphanyl)benzaldehyde benzoylhydrazonato)PdMe

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Technology Process of (2-(diphenylphosphanyl)benzaldehyde benzoylhydrazonato)PdMe

There total 3 articles about (2-(diphenylphosphanyl)benzaldehyde benzoylhydrazonato)PdMe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 422313-58-4
(2-(diphenylphosphanyl)benzaldehyde benzoylhydrazone)PdMe(Cl)

: 422313-59-5
(2-(diphenylphosphanyl)benzaldehyde benzoylhydrazonato)PdMe

Guidance literature:: With Et₃N; In tetrahydrofuran; byproducts: [Et3NH]Cl; under N2, excess of Et3N was added to THF soln. of complex, stirring at room temp. for 3 h; soln. was filtered, concd., Et2O was added, cooling to -20 °C overnight., solid was filtered off, washed with Et2O, dried in vac., elem. anal.;

Reference yield: 48.0%

: chloromethyl(1,5-cyclooctadiene)palladium(II)

: 238433-65-3
2-(2-(diphenylphosphino)benzylidene)benzoic acid hydrazone

: 422313-59-5
(2-(diphenylphosphanyl)benzaldehyde benzoylhydrazonato)PdMe

Guidance literature:: With Et₃N; In tetrahydrofuran; byproducts: [Et3NH]Cl; under N2, excess of Et3N was added to THF soln. of phosphine, Pd-complexwas added, (HNEt3)Cl was pptd., stirring at room temp. for 3 h; soln. was filtered, concd., Et2O was added, cooling to -20 °C overnight., solid was filtered off, washed with Et2O, dried in vac.;

Reference yield:

: 238433-65-3
2-(2-(diphenylphosphino)benzylidene)benzoic acid hydrazone

: 422313-59-5
(2-(diphenylphosphanyl)benzaldehyde benzoylhydrazonato)PdMe

Guidance literature:: Multi-step reaction with 2 steps

1: dichloromethane

2: Et₃N / tetrahydrofuran

With Et₃N; In tetrahydrofuran; dichloromethane;