6,7,8-trimethoxy-1-(4-nitrophenyl)-3,4-dihydroisoquinoline hydrochloride

Base Information

Chemical Name:6,7,8-trimethoxy-1-(4-nitrophenyl)-3,4-dihydroisoquinoline hydrochloride
CAS No.:1383540-88-2
Molecular Formula:C₁₈H₁₈N₂O₅*ClH
Molecular Weight:378.812
Hs Code.:

Synonyms:6,7,8-trimethoxy-1-(4-nitrophenyl)-3,4-dihydroisoquinoline hydrochloride

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Chemical Property of 6,7,8-trimethoxy-1-(4-nitrophenyl)-3,4-dihydroisoquinoline hydrochloride

Chemical Property:

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Technology Process of 6,7,8-trimethoxy-1-(4-nitrophenyl)-3,4-dihydroisoquinoline hydrochloride

There total 4 articles about 6,7,8-trimethoxy-1-(4-nitrophenyl)-3,4-dihydroisoquinoline hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 937617-05-5
C₁₈H₂₀N₂O₆

: 1383540-88-2
6,7,8-trimethoxy-1-(4-nitrophenyl)-3,4-dihydroisoquinoline hydrochloride

Guidance literature:: With trichlorophosphate; In acetonitrile; for 4h; Reflux;
DOI:10.1002/ardp.201100169

Reference yield:

: 6316-70-7
3,4,5-trimethoxy-β-nitrostyrene

: 1383540-88-2
6,7,8-trimethoxy-1-(4-nitrophenyl)-3,4-dihydroisoquinoline hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 5 h / Cooling with ice; Reflux

2.1: triethylamine / dichloromethane / 0.5 h / 20 °C

2.2: 4 h / 20 °C

3.1: trichlorophosphate / acetonitrile / 4 h / Reflux

With lithium aluminium tetrahydride; triethylamine; trichlorophosphate; In tetrahydrofuran; dichloromethane; acetonitrile;
DOI:10.1002/ardp.201100169

Reference yield:

: 832-92-8
mescaline hydrochloride

: 1383540-88-2
6,7,8-trimethoxy-1-(4-nitrophenyl)-3,4-dihydroisoquinoline hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 0.5 h / 20 °C

1.2: 4 h / 20 °C

2.1: trichlorophosphate / acetonitrile / 4 h / Reflux

With triethylamine; trichlorophosphate; In dichloromethane; acetonitrile;
DOI:10.1002/ardp.201100169