(1R,5R,6R)-2-(5-isopropyl-2-methyl-6-triethylsilanyloxymethylcyclohex-2-enyl)-N-methoxy-N-methylacetamide

Base Information

Chemical Name:(1R,5R,6R)-2-(5-isopropyl-2-methyl-6-triethylsilanyloxymethylcyclohex-2-enyl)-N-methoxy-N-methylacetamide
CAS No.:1027570-52-0
Molecular Formula:C₂₁H₄₁NO₃Si
Molecular Weight:383.647
Hs Code.:

Synonyms:(1R,5R,6R)-2-(5-isopropyl-2-methyl-6-triethylsilanyloxymethylcyclohex-2-enyl)-N-methoxy-N-methylacetamide

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Chemical Property of (1R,5R,6R)-2-(5-isopropyl-2-methyl-6-triethylsilanyloxymethylcyclohex-2-enyl)-N-methoxy-N-methylacetamide

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Technology Process of (1R,5R,6R)-2-(5-isopropyl-2-methyl-6-triethylsilanyloxymethylcyclohex-2-enyl)-N-methoxy-N-methylacetamide

There total 3 articles about (1R,5R,6R)-2-(5-isopropyl-2-methyl-6-triethylsilanyloxymethylcyclohex-2-enyl)-N-methoxy-N-methylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 79271-56-0
triethylsilyl trifluoromethyl sulfonate

: 1026090-92-5
(1R,5R,6R)-2-(6-hydroxymethyl-5-isopropyl-2-methylcyclohex-2-enyl)-N-methoxy-N-methylacetamide

: 1027570-52-0
(1R,5R,6R)-2-(5-isopropyl-2-methyl-6-triethylsilanyloxymethylcyclohex-2-enyl)-N-methoxy-N-methylacetamide

Guidance literature:: With 2,6-dimethylpyridine; In dichloromethane; at 0 ℃; for 2h;
DOI:10.1039/b207800g

Reference yield:

: 1027079-96-4
(4aR,8R,8aR)-8-isopropyl-5-methyl-1,4,4a,7,8,8a-hexahydroisochromen-3-one

: 1027570-52-0
(1R,5R,6R)-2-(5-isopropyl-2-methyl-6-triethylsilanyloxymethylcyclohex-2-enyl)-N-methoxy-N-methylacetamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: Me₃Al / hexane; toluene / 2 h / 20 °C

1.2: 94 percent / hexane; toluene / 2 h / 20 °C

2.1: 72 percent / 2,6-lutidine / CH₂Cl₂ / 2 h / 0 °C

With 2,6-dimethylpyridine; trimethylaluminum; In hexane; dichloromethane; toluene;
DOI:10.1039/b207800g

Reference yield:

: (3R,3aR,7aR)-3-isopropyl-7b-methyloctahydro-1,5-dioxacyclopropa[α]naphthalen-6-one

: 1027570-52-0
(1R,5R,6R)-2-(5-isopropyl-2-methyl-6-triethylsilanyloxymethylcyclohex-2-enyl)-N-methoxy-N-methylacetamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 86 percent / Zn; NaI; NaOAc / CH₂Cl₂; acetic acid / 96 h / 20 °C

2.1: Me₃Al / hexane; toluene / 2 h / 20 °C

2.2: 94 percent / hexane; toluene / 2 h / 20 °C

3.1: 72 percent / 2,6-lutidine / CH₂Cl₂ / 2 h / 0 °C

With 2,6-dimethylpyridine; trimethylaluminum; sodium acetate; sodium iodide; zinc; In hexane; dichloromethane; acetic acid; toluene;
DOI:10.1039/b207800g