1,1'-(1,2-ethanediyl)bis(1,2,3,4-tetrahydro-4,4-dimethyl-1-phenylphosphinolinium bis

Base Information

Chemical Name:1,1'-(1,2-ethanediyl)bis(1,2,3,4-tetrahydro-4,4-dimethyl-1-phenylphosphinolinium bis
CAS No.:81195-05-3
Molecular Formula:C₃₆H₄₂P₂*2F₆P
Molecular Weight:826.605
Hs Code.:

1,1'-(1,2-ethanediyl)bis(1,2,3,4-tetrahydro-4,4-dimethyl-1-phenylphosphinolinium bis<hexafluorophosphate(1-)>

Synonyms:1,1'-(1,2-ethanediyl)bis(1,2,3,4-tetrahydro-4,4-dimethyl-1-phenylphosphinolinium bis

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1'-(1,2-ethanediyl)bis(1,2,3,4-tetrahydro-4,4-dimethyl-1-phenylphosphinolinium bis

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Technology Process of 1,1'-(1,2-ethanediyl)bis(1,2,3,4-tetrahydro-4,4-dimethyl-1-phenylphosphinolinium bis

There total 3 articles about 1,1'-(1,2-ethanediyl)bis(1,2,3,4-tetrahydro-4,4-dimethyl-1-phenylphosphinolinium bis which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 81194-90-3
C₃₆H₄₂P₂⁽²⁺⁾*2Cl^(1-)

: 81195-05-3
1,1'-(1,2-ethanediyl)bis(1,2,3,4-tetrahydro-4,4-dimethyl-1-phenylphosphinolinium bis

Guidance literature:: With potassium hexafluorophosphate; PPA; 1.) 180 deg C, 1 h;
DOI:10.1021/ja00375a028

Reference yield:

: 1663-45-2
1,2-bis-(diphenylphosphino)ethane

: 81195-05-3
1,1'-(1,2-ethanediyl)bis(1,2,3,4-tetrahydro-4,4-dimethyl-1-phenylphosphinolinium bis

Guidance literature:: Multi-step reaction with 2 steps

1: benzene / 40 h / Heating

2: 40 percent / 1.) 115percent polyphosphoric acid, 2.) aq. KPF₆ / 1.) 180 deg C, 1 h

With potassium hexafluorophosphate; PPA; In benzene;
DOI:10.1021/ja00375a028

Reference yield:

: 503-60-6
3,3-dimethyl-allyl chloride

: 81195-05-3
1,1'-(1,2-ethanediyl)bis(1,2,3,4-tetrahydro-4,4-dimethyl-1-phenylphosphinolinium bis

Guidance literature:: Multi-step reaction with 2 steps

1: benzene / 40 h / Heating

2: 40 percent / 1.) 115percent polyphosphoric acid, 2.) aq. KPF₆ / 1.) 180 deg C, 1 h

With potassium hexafluorophosphate; PPA; In benzene;
DOI:10.1021/ja00375a028