ethyl N-(3-phenylprop-2-enyl)-N-tosylglycinate

Base Information

Chemical Name:ethyl N-(3-phenylprop-2-enyl)-N-tosylglycinate
CAS No.:79807-46-8
Molecular Formula:C₂₀H₂₃NO₄S
Molecular Weight:373.473
Hs Code.:

Synonyms:ethyl N-(3-phenylprop-2-enyl)-N-tosylglycinate

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Chemical Property of ethyl N-(3-phenylprop-2-enyl)-N-tosylglycinate

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Technology Process of ethyl N-(3-phenylprop-2-enyl)-N-tosylglycinate

There total 1 articles about ethyl N-(3-phenylprop-2-enyl)-N-tosylglycinate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 137845-37-5,144381-72-6,51985-30-9
4-methyl-N-(3-phenylallylidene)benzenesulfonamide

: 79807-46-8
ethyl N-(3-phenylprop-2-enyl)-N-tosylglycinate

Guidance literature:: Multi-step reaction with 2 steps

1: 82 percent / sodium borohydride / methanol; tetrahydrofuran / 2 h / 25 °C

2: 77 percent / K₂CO₃ / acetone / 16 h / Heating

With sodium tetrahydroborate; potassium carbonate; In tetrahydrofuran; methanol; acetone;
DOI:10.1039/P19810002443

Reference yield: 94.0%

: 79807-46-8
ethyl N-(3-phenylprop-2-enyl)-N-tosylglycinate

: 79807-47-9
N-(3-phenylprop-2-enyl)-N-tosylglycine

Guidance literature:: With sodium hydroxide; In methanol; for 3h; Heating;
DOI:10.1039/P19810002443

Reference yield:

: 79807-46-8
ethyl N-(3-phenylprop-2-enyl)-N-tosylglycinate

: 79807-34-4
N-(3-phenyl-propyl)-N-(toluene-4-sulfonyl)-glycine

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / aq. NaOH / methanol / 3 h / Heating

2: 80 percent / H₂ / 10percent palladium-on-carbone / ethanol / 1 h / 735.5 Torr

With sodium hydroxide; hydrogen; palladium on activated charcoal; In methanol; ethanol;
DOI:10.1039/P19810002443