C₂₁H₂₆BrNO₅

Base Information

Chemical Name:C₂₁H₂₆BrNO₅
CAS No.:1613702-47-8
Molecular Formula:C₂₁H₂₆BrNO₅
Molecular Weight:452.345
Hs Code.:

C<sub>21</sub>H<sub>26</sub>BrNO<sub>5</sub>

Synonyms:C₂₁H₂₆BrNO₅

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Chemical Property of C₂₁H₂₆BrNO₅

Chemical Property:

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Technology Process of C₂₁H₂₆BrNO₅

There total 3 articles about C₂₁H₂₆BrNO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 884320-42-7
2-(2-bromo-5-methoxyphenyl)prop-2-en-1-ol

: 1431854-35-1
tert-butyl ((2-hydroxy-5-oxocyclopent-1-en-1-yl)methyl)carbamate

: 1613702-47-8
C₂₁H₂₆BrNO₅

Guidance literature:: 2-(2-bromo-5-methoxyphenyl)prop-2-en-1-ol; With triethyl borane; palladium diacetate; triphenylphosphine; In tetrahydrofuran; hexane; at 20 ℃; for 3h; Inert atmosphere;

tert-butyl ((2-hydroxy-5-oxocyclopent-1-en-1-yl)methyl)carbamate; In tetrahydrofuran; hexane; for 18h;

Reference yield:

: 4248-19-5
tert-butyl carbazate

: 1613702-47-8
C₂₁H₂₆BrNO₅

Guidance literature:: Multi-step reaction with 3 steps

1.1: formic acid / water; methanol / 240 h / Inert atmosphere

2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 21.28 h / Inert atmosphere

3.1: palladium diacetate; triphenylphosphine; triethyl borane / tetrahydrofuran; hexane / 3 h / 20 °C / Inert atmosphere

3.2: 18 h

With formic acid; triethyl borane; palladium diacetate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triphenylphosphine; In tetrahydrofuran; methanol; hexane; water;

Reference yield:

: 1242161-32-5
tert-butyl ((phenylsulfonyl)methyl)carbamate

: 1613702-47-8
C₂₁H₂₆BrNO₅

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 21.28 h / Inert atmosphere

2.1: palladium diacetate; triphenylphosphine; triethyl borane / tetrahydrofuran; hexane / 3 h / 20 °C / Inert atmosphere

2.2: 18 h

With triethyl borane; palladium diacetate; 1,8-diazabicyclo[5.4.0]undec-7-ene; triphenylphosphine; In tetrahydrofuran; hexane;