p-Methoxyphenyl O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzoyl-4-O-(1-fluoro-1,1,3,3-tetraisopropyl-1,3-disiloxane-3-yl)-β-D-glucopyranoside

Base Information

Chemical Name:p-Methoxyphenyl O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzoyl-4-O-(1-fluoro-1,1,3,3-tetraisopropyl-1,3-disiloxane-3-yl)-β-D-glucopyranoside
CAS No.:155195-00-9
Molecular Formula:C₅₃H₇₁FO₁₉Si₂
Molecular Weight:1087.3
Hs Code.:

p-Methoxyphenyl O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzoyl-4-O-(1-fluoro-1,1,3,3-tetraisopropyl-1,3-disiloxane-3-yl)-β-D-glucopyranoside

Synonyms:p-Methoxyphenyl O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzoyl-4-O-(1-fluoro-1,1,3,3-tetraisopropyl-1,3-disiloxane-3-yl)-β-D-glucopyranoside

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Chemical Property of p-Methoxyphenyl O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzoyl-4-O-(1-fluoro-1,1,3,3-tetraisopropyl-1,3-disiloxane-3-yl)-β-D-glucopyranoside

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Technology Process of p-Methoxyphenyl O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzoyl-4-O-(1-fluoro-1,1,3,3-tetraisopropyl-1,3-disiloxane-3-yl)-β-D-glucopyranoside

There total 5 articles about p-Methoxyphenyl O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzoyl-4-O-(1-fluoro-1,1,3,3-tetraisopropyl-1,3-disiloxane-3-yl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 155194-83-5
p-Methoxyphenyl 2,3-di-O-benzoyl-4,6-O-(1,1,3,3-tetraisopropyl-1,3-disiloxane-1,3-diyl)-β-D-glucopyranoside

: 439-03-2,439-04-3,439-05-4,2823-44-1,2823-46-3,3934-29-0,4163-44-4,4163-45-5,20409-31-8,23235-96-3,51897-75-7,51897-76-8,51897-77-9,57573-38-3,62561-28-8,126641-47-2
2,3,4,6-tetra-O-acetyl-1-fluoro-α-D-glucopyranose

: 155195-00-9
p-Methoxyphenyl O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzoyl-4-O-(1-fluoro-1,1,3,3-tetraisopropyl-1,3-disiloxane-3-yl)-β-D-glucopyranoside

Guidance literature:: boron trifluoride diethyl etherate; In dichloromethane; for 14h; Ambient temperature;

Reference yield:

: 618-32-6
Benzoyl bromide

: 155195-00-9
p-Methoxyphenyl O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzoyl-4-O-(1-fluoro-1,1,3,3-tetraisopropyl-1,3-disiloxane-3-yl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / pyridine / 1.) r.t., 24 h, 2.) 60 deg C, 5 h

2: 68 percent / BF₃*Et₂O / CH₂Cl₂ / 14 h / Ambient temperature

With pyridine; boron trifluoride diethyl etherate; In dichloromethane;

Reference yield:

: 69304-37-6
1,3-Dichloro-1,1,3,3-tetraisopropyldisiloxane

: 155195-00-9
p-Methoxyphenyl O-(2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl)-(1->6)-2,3-di-O-benzoyl-4-O-(1-fluoro-1,1,3,3-tetraisopropyl-1,3-disiloxane-3-yl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / imidazole / dimethylformamide / 1 h / Ambient temperature

2: 100 percent / pyridine / 1.) r.t., 24 h, 2.) 60 deg C, 5 h

3: 68 percent / BF₃*Et₂O / CH₂Cl₂ / 14 h / Ambient temperature

With pyridine; 1H-imidazole; boron trifluoride diethyl etherate; In dichloromethane; N,N-dimethyl-formamide;