((2R,3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-carbamic acid allyl ester

Base Information

• Chemical Name: ((2R,3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-carbamic acid allyl ester
• CAS No.: 566200-25-7
• Molecular Formula: C₃₈H₄₁NO₇
• Molecular Weight: 623.746

Synonyms:((2R,3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-carbamic acid allyl ester

Chemical Property of ((2R,3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-carbamic acid allyl ester

Chemical Property:

Purity/Quality:

98% ^*data from raw suppliers

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Technology Process of ((2R,3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-carbamic acid allyl ester

There total 9 articles about ((2R,3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-carbamic acid allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

2,3,4,6-Tetra-O-benzyl-D-glucopyranose (4291-69-4,6386-24-9,6564-72-3,59531-24-7,69257-52-9,78184-89-1,78609-16-2,78609-17-3,78609-18-4,96553-53-6,104111-61-7,131347-08-5,4132-28-9) + C10H20N2O4S (439585-15-6) → ((2R,3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-carbamic acid allyl ester (566200-25-7)

Guidance literature:

In tetrahydrofuran; dichloromethane; for 6h; Heating;

DOI:10.1021/ja049293c

Reference yield: 76.0%

C44H44N2O11S → ((2R,3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-carbamic acid allyl ester (566200-25-7)

Guidance literature:

With potassium carbonate; thiophenol; In N,N-dimethyl-formamide;

DOI:10.1039/c9sc00857h

Reference yield:

C45H47NO8 → ((2R,3R,4S,5R,6R)-3,4,5-Tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl)-carbamic acid allyl ester (566200-25-7)

Guidance literature:

With methanol; samarium diiodide; In tetrahydrofuran; at 20 ℃; for 0.166667h;

DOI:10.1016/S0040-4039(03)00473-8

upstream raw materials:

2,3,4,6-Tetra-O-benzyl-D-glucopyranose

C₁₀H₂₀N₂O₄S

2,3,4,6-tetra-O-benzyl-D-glucopyranosyl fluoride

2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyl trichloroacetimidate

Downstream raw materials:

1-amino-2,3,4,6-tetra-O-benzyl-1-deoxy-β-D-glucopyranose

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