N-methyl-N-[2-(6-oxocyclohex-1-enyl)ethyl]-2,4-dinitrobenzenesulfonamide

Base Information

Chemical Name:N-methyl-N-[2-(6-oxocyclohex-1-enyl)ethyl]-2,4-dinitrobenzenesulfonamide
CAS No.:1257051-33-4
Molecular Formula:C₁₅H₁₇N₃O₇S
Molecular Weight:383.382
Hs Code.:

Synonyms:N-methyl-N-[2-(6-oxocyclohex-1-enyl)ethyl]-2,4-dinitrobenzenesulfonamide

Suppliers and Price of N-methyl-N-[2-(6-oxocyclohex-1-enyl)ethyl]-2,4-dinitrobenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-methyl-N-[2-(6-oxocyclohex-1-enyl)ethyl]-2,4-dinitrobenzenesulfonamide

Chemical Property:

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Technology Process of N-methyl-N-[2-(6-oxocyclohex-1-enyl)ethyl]-2,4-dinitrobenzenesulfonamide

There total 4 articles about N-methyl-N-[2-(6-oxocyclohex-1-enyl)ethyl]-2,4-dinitrobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1257051-32-3
N-(3-cyclopentenylpropyl)-N-methyl-2,4-dinitrobenzenesulfonamide

: 1257051-33-4
N-methyl-N-[2-(6-oxocyclohex-1-enyl)ethyl]-2,4-dinitrobenzenesulfonamide

Guidance literature:: N-(3-cyclopentenylpropyl)-N-methyl-2,4-dinitrobenzenesulfonamide; With ozone; In toluene; at 0 ℃;

With triphenylphosphine; In toluene; at 20 ℃; for 0.5h;

With trifluoroacetic acid; In water; toluene; at 80 ℃; for 2h;
DOI:10.1002/asia.201000458

Reference yield:

: 1257051-31-2
3-cyclopentenylpropyl methanesulfonate

: 1257051-33-4
N-methyl-N-[2-(6-oxocyclohex-1-enyl)ethyl]-2,4-dinitrobenzenesulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: methanol / 3 h / Reflux

2.1: sodium hydrogencarbonate / dichloromethane; water / 0.5 h / 20 °C

3.1: ozone / toluene / 0 °C

3.2: 0.5 h / 20 °C

3.3: 2 h / 80 °C

With sodium hydrogencarbonate; ozone; In methanol; dichloromethane; water; toluene; 3.3: Aldol condensation;
DOI:10.1002/asia.201000458

Reference yield:

: C₉H₁₇N

: 1257051-33-4
N-methyl-N-[2-(6-oxocyclohex-1-enyl)ethyl]-2,4-dinitrobenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydrogencarbonate / dichloromethane; water / 0.5 h / 20 °C

2.1: ozone / toluene / 0 °C

2.2: 0.5 h / 20 °C

2.3: 2 h / 80 °C

With sodium hydrogencarbonate; ozone; In dichloromethane; water; toluene; 2.3: Aldol condensation;
DOI:10.1002/asia.201000458