C₂₇H₃₃NO₅

Base Information

Chemical Name:C₂₇H₃₃NO₅
CAS No.:1315606-57-5
Molecular Formula:C₂₇H₃₃NO₅
Molecular Weight:451.563
Hs Code.:

C<sub>27</sub>H<sub>33</sub>NO<sub>5</sub>

Synonyms:C₂₇H₃₃NO₅

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Chemical Property of C₂₇H₃₃NO₅

Chemical Property:

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Technology Process of C₂₇H₃₃NO₅

There total 6 articles about C₂₇H₃₃NO₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1315606-48-4
C₂₄H₂₉NO₄

: 21204-67-1,2605-67-6
methyl (triphenylphosphoranylidene)acetate

: 1315606-57-5
C₂₇H₃₃NO₅

Guidance literature:: In benzene; at 20 ℃; for 16h; optical yield given as %de; stereoselective reaction; Inert atmosphere;
DOI:10.1021/ol201704g

Reference yield:

: 1315606-53-1
C₆H₁₁BrMg

: 1315606-57-5
C₂₇H₃₃NO₅

Guidance literature:: Multi-step reaction with 6 steps

1: tetrahydrofuran; toluene / 3.5 h / -78 °C / Inert atmosphere

2: hydrogenchloride; water / methanol / 2 h

3: potassium carbonate / water; acetone; toluene / 1 h / 20 °C

4: Hoveyda-Grubbs catalyst second generation / dichloromethane / 1 h / 20 °C / Inert atmosphere

5: boron trifluoride diethyl etherate / acetonitrile / 1 h / 20 °C / Inert atmosphere

6: benzene / 16 h / 20 °C / Inert atmosphere

With hydrogenchloride; Hoveyda-Grubbs catalyst second generation; boron trifluoride diethyl etherate; water; potassium carbonate; In tetrahydrofuran; methanol; dichloromethane; water; acetone; toluene; acetonitrile; benzene; 1: Grignard addition / 5: Michael addition;
DOI:10.1021/ol201704g

Reference yield:

: 944814-28-2
(S)-N-(2-(benzyloxy)ethylidene)-2-methylpropane-2-sulfinamide

: 1315606-57-5
C₂₇H₃₃NO₅

Guidance literature:: Multi-step reaction with 6 steps

1: tetrahydrofuran; toluene / 3.5 h / -78 °C / Inert atmosphere

2: hydrogenchloride; water / methanol / 2 h

3: potassium carbonate / water; acetone; toluene / 1 h / 20 °C

4: Hoveyda-Grubbs catalyst second generation / dichloromethane / 1 h / 20 °C / Inert atmosphere

5: boron trifluoride diethyl etherate / acetonitrile / 1 h / 20 °C / Inert atmosphere

6: benzene / 16 h / 20 °C / Inert atmosphere

With hydrogenchloride; Hoveyda-Grubbs catalyst second generation; boron trifluoride diethyl etherate; water; potassium carbonate; In tetrahydrofuran; methanol; dichloromethane; water; acetone; toluene; acetonitrile; benzene; 1: Grignard addition / 5: Michael addition;
DOI:10.1021/ol201704g