6-(tert-Butyl-diphenyl-silanyloxy)-3-oxo-2-(triphenyl-λ⁵-phosphanylidene)-hexanoic acid tert-butyl ester

Base Information

• Chemical Name: 6-(tert-Butyl-diphenyl-silanyloxy)-3-oxo-2-(triphenyl-λ⁵-phosphanylidene)-hexanoic acid tert-butyl ester
• CAS No.: 145237-24-7
• Molecular Formula: C₄₄H₄₉O₄PSi
• Molecular Weight: 700.93

Synonyms:6-(tert-Butyl-diphenyl-silanyloxy)-3-oxo-2-(triphenyl-λ⁵-phosphanylidene)-hexanoic acid tert-butyl ester

Chemical Property of 6-(tert-Butyl-diphenyl-silanyloxy)-3-oxo-2-(triphenyl-λ⁵-phosphanylidene)-hexanoic acid tert-butyl ester

Chemical Property:

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Technology Process of 6-(tert-Butyl-diphenyl-silanyloxy)-3-oxo-2-(triphenyl-λ⁵-phosphanylidene)-hexanoic acid tert-butyl ester

There total 1 articles about 6-(tert-Butyl-diphenyl-silanyloxy)-3-oxo-2-(triphenyl-λ⁵-phosphanylidene)-hexanoic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

(tert-Butoxycarbonylmethylene)triphenylphosphorane (86302-43-4,35000-38-5) + 4-((tert-butyldiphenylsilyl)oxy)butanoic acid (118715-16-5) → 6-(tert-Butyl-diphenyl-silanyloxy)-3-oxo-2-(triphenyl-λ5-phosphanylidene)-hexanoic acid tert-butyl ester (145237-24-7)

Guidance literature:

With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; Ambient temperature;

DOI:10.1016/S0040-4039(00)61111-5

upstream raw materials:

(tert-Butoxycarbonylmethylene)triphenylphosphorane

4-((tert-butyldiphenylsilyl)oxy)butanoic acid

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