bis(ethylenebis(diphenylphosphine))(2-n-octyldiazenido-N)iodomolybdenum

Base Information

Chemical Name:bis(ethylenebis(diphenylphosphine))(2-n-octyldiazenido-N)iodomolybdenum
CAS No.:59930-49-3
Molecular Formula:C₆₀H₆₅IMoN₂P₄
Molecular Weight:1160.93
Hs Code.:

Synonyms:bis(ethylenebis(diphenylphosphine))(2-n-octyldiazenido-N)iodomolybdenum

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Chemical Property of bis(ethylenebis(diphenylphosphine))(2-n-octyldiazenido-N)iodomolybdenum

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Technology Process of bis(ethylenebis(diphenylphosphine))(2-n-octyldiazenido-N)iodomolybdenum

There total 1 articles about bis(ethylenebis(diphenylphosphine))(2-n-octyldiazenido-N)iodomolybdenum which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 50495-19-7,25145-64-6,41700-58-7
[Mo(N₂)2(1,2-bis(diphenylphosphino)ethane)2]

: 629-27-6
1-Iodooctane

: 59930-49-3
bis(ethylenebis(diphenylphosphine))(2-n-octyldiazenido-N)iodomolybdenum

Guidance literature:: In benzene; Irradiation (UV/VIS); under N2 atm. n-octyl iodide added to soln. Mo(N2)2(dppe)2 in benzene and stirred at room temp. for 20 h under room fluorescent lighting; mixt. filtered, volume filtrate reduced and heptane added, ppt. filtered, filtrate volume reduced, solid crystd. by dissolving in benzene and adding heptane, volume reduced, product filtered, washed with heptane anddried in vacuo; elem. anal.;
DOI:10.1021/ic50215a007

Reference yield: 59.0%

: 59930-49-3
bis(ethylenebis(diphenylphosphine))(2-n-octyldiazenido-N)iodomolybdenum

: 59930-50-6
bis(ethylenebis(diphenylphosphine))iodo(2-n-octylhydrazido^(2-)-N)molybdenum chloride

Guidance literature:: With hydrogenchloride; In benzene; anhyd. HCl bubbled through benzene soln. MoI(N2C8H17)(dppe)2 for 0.33 h; soln. filtered, filtrate reduced and heptane added slowly with stirringand mixt. allowed to stand for 1.5 h, crystals filtered off,washed withheptane and dried in vacuo; elem. anal.;
DOI:10.1021/ic50215a007