N,N-dibenzyl-4-amino-3(S)-N-(boc)-aminobutanoic acid 4-tert-butyl ester

Base Information

Chemical Name:N,N-dibenzyl-4-amino-3(S)-N-(boc)-aminobutanoic acid 4-tert-butyl ester
CAS No.:1361253-46-4
Molecular Formula:C₂₇H₃₈N₂O₄
Molecular Weight:454.61
Hs Code.:

Synonyms:N,N-dibenzyl-4-amino-3(S)-N-(boc)-aminobutanoic acid 4-tert-butyl ester

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Chemical Property of N,N-dibenzyl-4-amino-3(S)-N-(boc)-aminobutanoic acid 4-tert-butyl ester

Chemical Property:

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Technology Process of N,N-dibenzyl-4-amino-3(S)-N-(boc)-aminobutanoic acid 4-tert-butyl ester

There total 2 articles about N,N-dibenzyl-4-amino-3(S)-N-(boc)-aminobutanoic acid 4-tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1361253-44-2
N,N-dibenzyl-L-N-(boc)-aspartamide 4-tert-butyl ester

: 1361253-46-4
N,N-dibenzyl-4-amino-3(S)-N-(boc)-aminobutanoic acid 4-tert-butyl ester

Guidance literature:: With diphenylsilane; dodecacarbonyl-triangulo-triruthenium; In tetrahydrofuran; for 40h; Reflux;

Reference yield:

: 1676-90-0
Boc-Asp(OtBu)-OH

: 103-49-1
dibenzylamine

: 1361253-46-4
N,N-dibenzyl-4-amino-3(S)-N-(boc)-aminobutanoic acid 4-tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / 0.5 h / -5 °C

1.2: 3 h

2.1: diphenylsilane / dodecacarbonyl-triangulo-triruthenium / tetrahydrofuran / 40 h / Reflux

With 4-methyl-morpholine; diphenylsilane; isobutyl chloroformate; dodecacarbonyl-triangulo-triruthenium; In tetrahydrofuran;