anhydroisolariciresinol dimethyl ether

Base Information

Chemical Name:anhydroisolariciresinol dimethyl ether
CAS No.:26194-59-2
Molecular Formula:C₂₂H₂₆O₅
Molecular Weight:370.445
Hs Code.:

Synonyms:anhydroisolariciresinol dimethyl ether

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Chemical Property of anhydroisolariciresinol dimethyl ether

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Technology Process of anhydroisolariciresinol dimethyl ether

There total 4 articles about anhydroisolariciresinol dimethyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21966-92-7
isolariciresinol dimethyl ether

: 26194-59-2
anhydroisolariciresinol dimethyl ether

Guidance literature:: With potassium hydrogensulfate; at 180 ℃;
DOI:10.1039/jr9500000071 DOI:10.1039/jr9370000384

Reference yield:

: 321747-11-9
[(1S,9R,12R)-1-(3,4-Dimethoxy-phenyl)-4,5-dimethoxy-11-oxa-tricyclo[7.2.1.0^2,7]dodeca-2⁽⁷⁾,3,5-trien-12-yl]-methanol

: 26194-59-2
anhydroisolariciresinol dimethyl ether

Guidance literature:: Multi-step reaction with 3 steps

1.1: 85 percent / DMAP / tetrahydrofuran / 2 h / 25 °C

2.1: H₂ / 10percent Pd/C / aq. ethanol / 24 h / 25 °C

2.2: MeOH; K₂CO₃ / 1.9 h / 25 °C

3.1: p-toluenesulfonyl chloride; pyridine / 3 h / Heating

With pyridine; dmap; hydrogen; p-toluenesulfonyl chloride; 10percent Pd/C; In tetrahydrofuran; ethanol;
DOI:10.1021/jm990563p

Reference yield:

: 321747-13-1
Acetic acid (1S,9R,12R)-1-(3,4-dimethoxy-phenyl)-4,5-dimethoxy-11-oxa-tricyclo[7.2.1.0^2,7]dodeca-2⁽⁷⁾,3,5-trien-12-ylmethyl ester

: 26194-59-2
anhydroisolariciresinol dimethyl ether

Guidance literature:: Multi-step reaction with 2 steps

1.1: H₂ / 10percent Pd/C / aq. ethanol / 24 h / 25 °C

1.2: MeOH; K₂CO₃ / 1.9 h / 25 °C

2.1: p-toluenesulfonyl chloride; pyridine / 3 h / Heating

With pyridine; hydrogen; p-toluenesulfonyl chloride; 10percent Pd/C; In ethanol;
DOI:10.1021/jm990563p