Technology Process of C23H25NO4
There total 4 articles about C23H25NO4 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
aluminum (III) chloride;
In
1,2-dichloro-ethane;
at 25 - 110 ℃;
for 0.05h;
under 12929 Torr;
Microwave irradiation;
DOI:10.1021/jm3013097
- Guidance literature:
-
Multi-step reaction with 2 steps
1: n-butyllithium / hexane; tetrahydrofuran / 14 h / -40 - 25 °C
2: aluminum (III) chloride / 1,2-dichloro-ethane / 0.05 h / 25 - 110 °C / 12929 Torr / Microwave irradiation
With
aluminum (III) chloride; n-butyllithium;
In
tetrahydrofuran; hexane; 1,2-dichloro-ethane;
DOI:10.1021/jm3013097
- Guidance literature:
-
Multi-step reaction with 3 steps
1: triethylamine / tetrahydrofuran / 12 h / 25 °C / Cooling with ice
2: n-butyllithium / hexane; tetrahydrofuran / 14 h / -40 - 25 °C
3: aluminum (III) chloride / 1,2-dichloro-ethane / 0.05 h / 25 - 110 °C / 12929 Torr / Microwave irradiation
With
aluminum (III) chloride; n-butyllithium; triethylamine;
In
tetrahydrofuran; hexane; 1,2-dichloro-ethane;
DOI:10.1021/jm3013097