Acetic acid (1S,2R,3S,4S,5R,6S)-3-acetoxy-4-acetylamino-5,6-bis-benzyloxy-2-nitro-cyclohexyl ester

Base Information

Chemical Name:Acetic acid (1S,2R,3S,4S,5R,6S)-3-acetoxy-4-acetylamino-5,6-bis-benzyloxy-2-nitro-cyclohexyl ester
CAS No.:69940-09-6
Molecular Formula:C₂₆H₃₀N₂O₉
Molecular Weight:514.532
Hs Code.:

Synonyms:Acetic acid (1S,2R,3S,4S,5R,6S)-3-acetoxy-4-acetylamino-5,6-bis-benzyloxy-2-nitro-cyclohexyl ester

Suppliers and Price of Acetic acid (1S,2R,3S,4S,5R,6S)-3-acetoxy-4-acetylamino-5,6-bis-benzyloxy-2-nitro-cyclohexyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Acetic acid (1S,2R,3S,4S,5R,6S)-3-acetoxy-4-acetylamino-5,6-bis-benzyloxy-2-nitro-cyclohexyl ester

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Hazard Codes:

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Technology Process of Acetic acid (1S,2R,3S,4S,5R,6S)-3-acetoxy-4-acetylamino-5,6-bis-benzyloxy-2-nitro-cyclohexyl ester

There total 9 articles about Acetic acid (1S,2R,3S,4S,5R,6S)-3-acetoxy-4-acetylamino-5,6-bis-benzyloxy-2-nitro-cyclohexyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 69940-08-5
N-((1S,2R,3R,4S,5R,6S)-2,3-Bis-benzyloxy-4,6-dihydroxy-5-nitro-cyclohexyl)-acetamide

: 108-24-7
acetic anhydride

: 69940-09-6
Acetic acid (1S,2R,3S,4S,5R,6S)-3-acetoxy-4-acetylamino-5,6-bis-benzyloxy-2-nitro-cyclohexyl ester

Guidance literature:: With boron trifluoride diethyl etherate; In diethyl ether;

Reference yield:

: 72-87-7,1136-42-1,1136-44-3,6082-29-7,6730-06-9,7772-94-3,10036-64-3,14131-60-3,14131-64-7,14131-68-1,14215-68-0,62057-49-2,62057-50-5,62057-51-6,62057-52-7,62057-53-8,62057-54-9,62057-55-0,62057-56-1,62075-50-7,62137-54-6,134451-97-1,134522-12-6,148347-16-4
N-acetyl-D-glucosamine

: 69940-09-6
Acetic acid (1S,2R,3S,4S,5R,6S)-3-acetoxy-4-acetylamino-5,6-bis-benzyloxy-2-nitro-cyclohexyl ester

Guidance literature:: Multi-step reaction with 8 steps

1: acetyl chloride

2: pyridine

3: NaOH

4: 5percent aq. H₂SO₄

5: CrO₃, aq. H₂SO₄

6: benzene

7: NaOMe / methanol

8: 100 percent / BF₃*Et₂O / diethyl ether

With pyridine; chromium(VI) oxide; sodium hydroxide; sulfuric acid; boron trifluoride diethyl etherate; sodium methylate; acetyl chloride; In methanol; diethyl ether; benzene;

Reference yield:

: 42756-57-0,50908-05-9,69892-34-8,78488-16-1,78488-31-0
methyl 2-acetamido-2-deoxy-6-O-trityl-D-glucopyranoside

: 69940-09-6
Acetic acid (1S,2R,3S,4S,5R,6S)-3-acetoxy-4-acetylamino-5,6-bis-benzyloxy-2-nitro-cyclohexyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: NaOH

2: 5percent aq. H₂SO₄

3: CrO₃, aq. H₂SO₄

4: benzene

5: NaOMe / methanol

6: 100 percent / BF₃*Et₂O / diethyl ether

With chromium(VI) oxide; sodium hydroxide; sulfuric acid; boron trifluoride diethyl etherate; sodium methylate; In methanol; diethyl ether; benzene;