2-(4-(4-(1-(4-chlorophenyl)cyclopropylamino)-6-(2,2,2-trifluoroethoxy-D₂)-1,3,5-triazin-2-ylamino)benzamido)-N,N,N-trimethylethanaminium

Base Information

• Chemical Name: 2-(4-(4-(1-(4-chlorophenyl)cyclopropylamino)-6-(2,2,2-trifluoroethoxy-D₂)-1,3,5-triazin-2-ylamino)benzamido)-N,N,N-trimethylethanaminium
• CAS No.: 1620775-30-5
• Molecular Formula: C₂₆H₃₀ClF₃N₇O₂
• Molecular Weight: 567.002

Synonyms:2-(4-(4-(1-(4-chlorophenyl)cyclopropylamino)-6-(2,2,2-trifluoroethoxy-D₂)-1,3,5-triazin-2-ylamino)benzamido)-N,N,N-trimethylethanaminium

Chemical Property of 2-(4-(4-(1-(4-chlorophenyl)cyclopropylamino)-6-(2,2,2-trifluoroethoxy-D₂)-1,3,5-triazin-2-ylamino)benzamido)-N,N,N-trimethylethanaminium

Chemical Property:

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Technology Process of 2-(4-(4-(1-(4-chlorophenyl)cyclopropylamino)-6-(2,2,2-trifluoroethoxy-D₂)-1,3,5-triazin-2-ylamino)benzamido)-N,N,N-trimethylethanaminium

There total 5 articles about 2-(4-(4-(1-(4-chlorophenyl)cyclopropylamino)-6-(2,2,2-trifluoroethoxy-D₂)-1,3,5-triazin-2-ylamino)benzamido)-N,N,N-trimethylethanaminium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-(4-(1-(4-chlorophenyl)cyclopropylamino)-6-(2,2,2-trifluoroethoxy-D2)-1,3,5-triazin-2-ylamino)benzoyl chloride (1620775-47-4) + 2-AMINOETHYL TRIMETHYLAMMONIUM CHLORIDE (10256-43-6) → 2-(4-(4-(1-(4-chlorophenyl)cyclopropylamino)-6-(2,2,2-trifluoroethoxy-D2)-1,3,5-triazin-2-ylamino)benzamido)-N,N,N-trimethylethanaminium (1620775-30-5)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; at 20 ℃; for 16h;

Reference yield:

C5(2)H2Cl2F3N3O (1620775-44-1) → 2-(4-(4-(1-(4-chlorophenyl)cyclopropylamino)-6-(2,2,2-trifluoroethoxy-D2)-1,3,5-triazin-2-ylamino)benzamido)-N,N,N-trimethylethanaminium (1620775-30-5)

Guidance literature:

Multi-step reaction with 5 steps

1.1: N-ethyl-N,N-diisopropylamine / 16 h / 20 °C

2.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 16 h / 70 °C

3.1: potassium carbonate / acetone; water / 16 h / 80 °C / Sealed tube

3.2: pH 2

4.1: sulfuryl dichloride / dichloromethane / 16 h / 90 °C / Sealed tube

5.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 16 h / 20 °C

With sulfuryl dichloride; potassium carbonate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; water; acetone;

Reference yield:

methyl 4-(4-chloro-6-(2,2,2-trifluoroethoxy-D2)-1,3,5-triazin-2-ylamino)benzoate (1620775-45-2) → 2-(4-(4-(1-(4-chlorophenyl)cyclopropylamino)-6-(2,2,2-trifluoroethoxy-D2)-1,3,5-triazin-2-ylamino)benzamido)-N,N,N-trimethylethanaminium (1620775-30-5)

Guidance literature:

Multi-step reaction with 4 steps

1.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 16 h / 70 °C

2.1: potassium carbonate / acetone; water / 16 h / 80 °C / Sealed tube

2.2: pH 2

3.1: sulfuryl dichloride / dichloromethane / 16 h / 90 °C / Sealed tube

4.1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 16 h / 20 °C

With sulfuryl dichloride; potassium carbonate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; water; acetone;

upstream raw materials:

C₅⁽²⁾H₂Cl₂F₃N₃O

methyl 4-(4-chloro-6-(2,2,2-trifluoroethoxy-D₂)-1,3,5-triazin-2-ylamino)benzoate

methyl 4-(4-(1-(4-chlorophenyl)cyclopropylamino)-6-(2,2,2-trifluoroethoxy-D₂)-1,3,5-triazin-2-ylamino)benzoate

4-(4-(1-(4-chlorophenyl)cyclopropylamino)-6-(2,2,2-trifluoroethoxy-D₂)-1,3,5-triazin-2-ylamino)benzoic acid

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