DL-2,2'-[6-(4-sulfamoylphenethylamino)-1,3,5-triazine-2,4-diyl]bis(azanediyl)dipropanoic acid

Base Information

Chemical Name:DL-2,2'-[6-(4-sulfamoylphenethylamino)-1,3,5-triazine-2,4-diyl]bis(azanediyl)dipropanoic acid
CAS No.:1311200-33-5
Molecular Formula:C₁₇H₂₃N₇O₆S
Molecular Weight:453.479
Hs Code.:

Synonyms:DL-2,2'-[6-(4-sulfamoylphenethylamino)-1,3,5-triazine-2,4-diyl]bis(azanediyl)dipropanoic acid

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Chemical Property of DL-2,2'-[6-(4-sulfamoylphenethylamino)-1,3,5-triazine-2,4-diyl]bis(azanediyl)dipropanoic acid

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Technology Process of DL-2,2'-[6-(4-sulfamoylphenethylamino)-1,3,5-triazine-2,4-diyl]bis(azanediyl)dipropanoic acid

There total 2 articles about DL-2,2'-[6-(4-sulfamoylphenethylamino)-1,3,5-triazine-2,4-diyl]bis(azanediyl)dipropanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 302-72-7,25191-17-7,18875-37-1
rac-Ala-OH

: 796871-27-7
4-{2-[(4,6-dichloro-1,3,5-triazin-2-yl)amino]ethyl}benzene-1-sulfonamide

: 1311200-33-5
DL-2,2'-[6-(4-sulfamoylphenethylamino)-1,3,5-triazine-2,4-diyl]bis(azanediyl)dipropanoic acid

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.bmc.2011.04.005

Reference yield:

: 35303-76-5
4-(2-aminoethyl)benzenesulfonamide

: 1311200-33-5
DL-2,2'-[6-(4-sulfamoylphenethylamino)-1,3,5-triazine-2,4-diyl]bis(azanediyl)dipropanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetone / 0 °C

1.2: 1.33 h

2.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 °C / Inert atmosphere

With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.bmc.2011.04.005