C₂₅H₂₉BrN₂O₇S

Base Information

Chemical Name:C₂₅H₂₉BrN₂O₇S
CAS No.:1094172-66-3
Molecular Formula:C₂₅H₂₉BrN₂O₇S
Molecular Weight:581.484
Hs Code.:

C<sub>25</sub>H<sub>29</sub>BrN<sub>2</sub>O<sub>7</sub>S

Synonyms:C₂₅H₂₉BrN₂O₇S

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Chemical Property of C₂₅H₂₉BrN₂O₇S

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Technology Process of C₂₅H₂₉BrN₂O₇S

There total 6 articles about C₂₅H₂₉BrN₂O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1094172-75-4
C₂₀H₂₁BrN₂O₅S

: 24424-99-5
di-tert-butyl dicarbonate

: 1094172-66-3
C₂₅H₂₉BrN₂O₇S

Guidance literature:: In dichloromethane; at 20 ℃; for 2h;
DOI:10.1016/j.tetlet.2008.10.020

Reference yield:

: C₁₃H₁₅BrN₂O₃

: 1094172-66-3
C₂₅H₂₉BrN₂O₇S

Guidance literature:: Multi-step reaction with 5 steps

1: acetic acid; zinc / water / 1.83 h / 80 - 85 °C

2: glyoxylic acid ethyl ester; magnesium sulfate / dichloromethane / 0 - 20 °C

3: dmap; triethylamine / toluene / 18 h / 70 °C

4: ammonium cerium (IV) nitrate / water; acetonitrile / 0.25 h / -15 °C

5: dichloromethane / 4 h / 20 °C

With dmap; glyoxylic acid ethyl ester; ammonium cerium (IV) nitrate; magnesium sulfate; acetic acid; triethylamine; zinc; In dichloromethane; water; toluene; acetonitrile;
DOI:10.1002/ejoc.201100242

Reference yield:

: 1094172-65-2
C₂₀H₂₁BrN₂O₄

: 1094172-66-3
C₂₅H₂₉BrN₂O₇S

Guidance literature:: Multi-step reaction with 3 steps

1: dmap; triethylamine / toluene / 18 h / 70 °C

2: ammonium cerium (IV) nitrate / water; acetonitrile / 0.25 h / -15 °C

3: dichloromethane / 4 h / 20 °C

With dmap; ammonium cerium (IV) nitrate; triethylamine; In dichloromethane; water; toluene; acetonitrile;
DOI:10.1002/ejoc.201100242