C₂₈H₅₀O₂Si₂

Base Information

Chemical Name:C₂₈H₅₀O₂Si₂
CAS No.:1521267-03-7
Molecular Formula:C₂₈H₅₀O₂Si₂
Molecular Weight:474.875
Hs Code.:

C<sub>28</sub>H<sub>50</sub>O<sub>2</sub>Si<sub>2</sub>

Synonyms:C₂₈H₅₀O₂Si₂

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Chemical Property of C₂₈H₅₀O₂Si₂

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Technology Process of C₂₈H₅₀O₂Si₂

There total 11 articles about C₂₈H₅₀O₂Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1521267-02-6
C₁₉H₃₆O₂Si

: 1631-70-5
benzyldimethylsilane

: 1521267-03-7
C₂₈H₅₀O₂Si₂

Guidance literature:: With tris(acetonitrile)pentamethylcyclopentadienylruthenium(II) hexafluorophosphate; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/jacs.6b05127

Reference yield:

: 1521267-02-6
C₁₉H₃₆O₂Si

: 1631-70-5
benzyldimethylsilane

: 1521267-03-7
C₂₈H₅₀O₂Si₂

: C₂₈H₅₀O₂Si₂

Guidance literature:: With tris(acetonitrile)pentamethylcyclopentadienylruthenium(II) hexafluorophosphate; In acetone; at -78 - -5 ℃; for 12.1h; Overall yield = 86 %; Overall yield = 2.51 g; diastereoselective reaction; Inert atmosphere;
DOI:10.1021/ja411270d

Reference yield:

: 80522-42-5
triisopropylsilyl trifluoromethanesulfonate

: 1521267-03-7
C₂₈H₅₀O₂Si₂

Guidance literature:: Multi-step reaction with 5 steps

1: 2,6-dimethylpyridine / Inert atmosphere

2: isopropylmagnesium chloride / Inert atmosphere

3: Inert atmosphere

4: benzo[1,3,2]dioxaborole; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole / 4 h / -78 °C / Inert atmosphere

5: tris(acetonitrile)pentamethylcyclopentadienylruthenium(II) hexafluorophosphate / Inert atmosphere

With 2,6-dimethylpyridine; tris(acetonitrile)pentamethylcyclopentadienylruthenium(II) hexafluorophosphate; isopropylmagnesium chloride; (S)-1-methyl-3,3-diphenyl-hexahydropyrrolo[1,2-c][1,3,2]oxazaborole; benzo[1,3,2]dioxaborole;
DOI:10.1021/jacs.6b05127