C₃₇H₅₂N₂O₄

Base Information

Chemical Name:C₃₇H₅₂N₂O₄
CAS No.:1220904-32-4
Molecular Formula:C₃₇H₅₂N₂O₄
Molecular Weight:588.831
Hs Code.:

C<sub>37</sub>H<sub>52</sub>N<sub>2</sub>O<sub>4</sub>

Synonyms:C₃₇H₅₂N₂O₄

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Chemical Property of C₃₇H₅₂N₂O₄

Chemical Property:

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Technology Process of C₃₇H₅₂N₂O₄

There total 11 articles about C₃₇H₅₂N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 1220904-29-9
C₃₀H₄₃F₃N₂O₆S

: 22237-13-4
(4-ethoxyphenyl)boronic acid

: 1220904-32-4
C₃₇H₅₂N₂O₄

Guidance literature:: With sodium carbonate; bis-triphenylphosphine-palladium(II) chloride; In 1,2-dimethoxyethane; water; at 70 ℃; for 3h;

Reference yield:

: 619-66-9
4-Carboxybenzaldehyde

: 1220904-32-4
C₃₇H₅₂N₂O₄

Guidance literature:: Multi-step reaction with 11 steps

1.1: potassium carbonate / N,N-dimethyl-formamide; tetrahydrofuran / 64 h / 70 °C

2.1: caesium carbonate / dichloromethane / 30 h / 42 °C

3.1: iodine; magnesium / diethyl ether / 2.75 h / Reflux; Inert atmosphere

3.2: 2 h / -78 - 20 °C

3.3: 0 °C

4.1: hydrogenchloride; methanol / 1,4-dioxane / 1.5 h / 20 °C

5.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 16.25 h / 0 - 20 °C

6.1: trifluoroacetic acid / dichloromethane / 4 h

7.1: triethylamine / isopropyl alcohol / 24 h / Reflux; Molecular sieve; Inert atmosphere

8.1: tert-butylhypochlorite / dichloromethane / 0.75 h

8.2: 0.75 h

9.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / 20 °C

10.1: N-ethyl-N,N-diisopropylamine / dichloromethane / -10 °C

11.1: sodium carbonate / bis-triphenylphosphine-palladium(II) chloride / 1,2-dimethoxyethane; water / 3 h / 70 °C

With hydrogenchloride; methanol; tert-butylhypochlorite; iodine; sodium carbonate; potassium carbonate; benzotriazol-1-ol; caesium carbonate; magnesium; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol;

Reference yield:

: 70240-29-8
4-(isopropyloxycarbonyl)benzaldehyde

: 1220904-32-4
C₃₇H₅₂N₂O₄

Guidance literature:: Multi-step reaction with 10 steps

1.1: caesium carbonate / dichloromethane / 30 h / 42 °C

2.1: iodine; magnesium / diethyl ether / 2.75 h / Reflux; Inert atmosphere

2.2: 2 h / -78 - 20 °C

2.3: 0 °C

3.1: hydrogenchloride; methanol / 1,4-dioxane / 1.5 h / 20 °C

4.1: N-ethyl-N,N-diisopropylamine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 16.25 h / 0 - 20 °C

5.1: trifluoroacetic acid / dichloromethane / 4 h

6.1: triethylamine / isopropyl alcohol / 24 h / Reflux; Molecular sieve; Inert atmosphere

7.1: tert-butylhypochlorite / dichloromethane / 0.75 h

7.2: 0.75 h

8.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 3 h / 20 °C

9.1: N-ethyl-N,N-diisopropylamine / dichloromethane / -10 °C

10.1: sodium carbonate / bis-triphenylphosphine-palladium(II) chloride / 1,2-dimethoxyethane; water / 3 h / 70 °C

With hydrogenchloride; methanol; tert-butylhypochlorite; iodine; sodium carbonate; benzotriazol-1-ol; caesium carbonate; magnesium; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; bis-triphenylphosphine-palladium(II) chloride; In 1,4-dioxane; 1,2-dimethoxyethane; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide; isopropyl alcohol;