C₄₁H₆₀O₄Si

Base Information

Chemical Name:C₄₁H₆₀O₄Si
CAS No.:1427556-14-6
Molecular Formula:C₄₁H₆₀O₄Si
Molecular Weight:645.01
Hs Code.:

C<sub>41</sub>H<sub>60</sub>O<sub>4</sub>Si

Synonyms:C₄₁H₆₀O₄Si

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Chemical Property of C₄₁H₆₀O₄Si

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Technology Process of C₄₁H₆₀O₄Si

There total 11 articles about C₄₁H₆₀O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₂H₄₄O₃Si

: 1427556-15-7
(E)-5-[(6-(methoxymethoxy)-5-methylhex-4-en-1-yl)sulfonyl]-1-phenyl-1H-tetrazole

: 1427556-14-6
C₄₁H₆₀O₄Si

: 1427556-25-9
C₄₁H₆₀O₄Si

Guidance literature:: With potassium hexamethylsilazane; In N,N-dimethyl-formamide; toluene; at -78 ℃; Overall yield = 338 mg; Inert atmosphere;
DOI:10.1016/j.tet.2013.02.062

Reference yield:

: 1427556-22-6
tert-butyl (2S,3S)-3-[(R)-2-methylpent-4-ynyl] oxiran-2-ylmethoxy diphenylsilane

: 1427556-14-6
C₄₁H₆₀O₄Si

: 1427556-25-9
C₄₁H₆₀O₄Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: palladium diacetate; triphenylphosphine / 1,2-dimethoxyethane / 168 h / 35 °C / Inert atmosphere

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran; dimethyl sulfoxide / 0.5 h / 20 - 80 °C / Inert atmosphere

3.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triphenyl-arsane / 1-methyl-pyrrolidin-2-one / 0.25 h / 20 °C / Inert atmosphere

3.2: 0.67 h / 35 °C / Inert atmosphere

4.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 1 h / 50 °C / Inert atmosphere

5.1: potassium hexamethylsilazane / N,N-dimethyl-formamide; toluene / -78 °C / Inert atmosphere

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triphenyl-arsane; tetrabutyl ammonium fluoride; palladium diacetate; potassium hexamethylsilazane; triphenylphosphine; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; 1,2-dimethoxyethane; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene; 3.1: |Stille Cross Coupling / 3.2: |Stille Cross Coupling / 5.1: |Julia-Kocienski Olefination;
DOI:10.1016/j.tet.2013.02.062

Reference yield:

: 1427556-23-7
C₃₆H₅₂O₂Si₂Sn

: 1427556-14-6
C₄₁H₆₀O₄Si

: 1427556-25-9
C₄₁H₆₀O₄Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: tetrabutyl ammonium fluoride / tetrahydrofuran; dimethyl sulfoxide / 0.5 h / 20 - 80 °C / Inert atmosphere

2.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triphenyl-arsane / 1-methyl-pyrrolidin-2-one / 0.25 h / 20 °C / Inert atmosphere

2.2: 0.67 h / 35 °C / Inert atmosphere

3.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 1 h / 50 °C / Inert atmosphere

4.1: potassium hexamethylsilazane / N,N-dimethyl-formamide; toluene / -78 °C / Inert atmosphere

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; triphenyl-arsane; tetrabutyl ammonium fluoride; potassium hexamethylsilazane; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; 1-methyl-pyrrolidin-2-one; dimethyl sulfoxide; N,N-dimethyl-formamide; toluene; 2.1: |Stille Cross Coupling / 2.2: |Stille Cross Coupling / 4.1: |Julia-Kocienski Olefination;
DOI:10.1016/j.tet.2013.02.062