tert-butyl (2S,5S)-6-amino-2-benzyloxycarbonylamino-5-[(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyloxy)-(1->2)-(3,4,6-tri-O-benzyl-β-D-galactopyranosyloxy)]hexanoate

Base Information

Chemical Name:tert-butyl (2S,5S)-6-amino-2-benzyloxycarbonylamino-5-[(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyloxy)-(1->2)-(3,4,6-tri-O-benzyl-β-D-galactopyranosyloxy)]hexanoate
CAS No.:1005413-40-0
Molecular Formula:C₇₉H₉₀N₂O₁₅
Molecular Weight:1307.59
Hs Code.:

tert-butyl (2S,5S)-6-amino-2-benzyloxycarbonylamino-5-[(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyloxy)-(1->2)-(3,4,6-tri-O-benzyl-β-D-galactopyranosyloxy)]hexanoate

Synonyms:tert-butyl (2S,5S)-6-amino-2-benzyloxycarbonylamino-5-[(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyloxy)-(1->2)-(3,4,6-tri-O-benzyl-β-D-galactopyranosyloxy)]hexanoate

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Chemical Property of tert-butyl (2S,5S)-6-amino-2-benzyloxycarbonylamino-5-[(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyloxy)-(1->2)-(3,4,6-tri-O-benzyl-β-D-galactopyranosyloxy)]hexanoate

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Technology Process of tert-butyl (2S,5S)-6-amino-2-benzyloxycarbonylamino-5-[(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyloxy)-(1->2)-(3,4,6-tri-O-benzyl-β-D-galactopyranosyloxy)]hexanoate

There total 1 articles about tert-butyl (2S,5S)-6-amino-2-benzyloxycarbonylamino-5-[(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyloxy)-(1->2)-(3,4,6-tri-O-benzyl-β-D-galactopyranosyloxy)]hexanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.0%

: 1005413-39-7
tert-butyl (2S)-6-azido-2-benzyloxycarbonylamino-5-[(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyloxy)-(1->2)-(3,4,6-tri-O-benzyl-β-D-galactopyranosyloxy)]hexanoate

: 1005413-40-0
tert-butyl (2S,5S)-6-amino-2-benzyloxycarbonylamino-5-[(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyloxy)-(1->2)-(3,4,6-tri-O-benzyl-β-D-galactopyranosyloxy)]hexanoate

: 862674-26-8
tert-butyl (2S,5R)-6-amino-2-benzyloxycarbonylamino-5-[(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyloxy)-(1->2)-(3,4,6-tri-O-benzyl-β-D-galactopyranosyloxy)]hexanoate

Guidance literature:: With thiophenol; triethylamine; tin(ll) chloride; In tetrahydrofuran; at 20 ℃; for 1h;
DOI:10.1016/j.tetasy.2007.10.037

Reference yield: 81.0%

: 1005413-40-0
tert-butyl (2S,5S)-6-amino-2-benzyloxycarbonylamino-5-[(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyloxy)-(1->2)-(3,4,6-tri-O-benzyl-β-D-galactopyranosyloxy)]hexanoate

: 76-05-1
trifluoroacetic acid

: (2S,5S)-2,6-diamino-5-[α-D-glucopyranosyl-(1->2)-β-D-galactopyranosyloxy]hexanoic acid ditrifluoroacetate

Guidance literature:: tert-butyl (2S,5S)-6-amino-2-benzyloxycarbonylamino-5-[(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyloxy)-(1->2)-(3,4,6-tri-O-benzyl-β-D-galactopyranosyloxy)]hexanoate; With hydrogen; palladium on activated charcoal; In tetrahydrofuran; ethanol; at 20 ℃; for 9h; under 760.051 Torr;

trifluoroacetic acid; In water; at 20 ℃; for 1h; Further stages.;
DOI:10.1016/j.tetasy.2007.10.037

Reference yield: 61.0%

: 1005413-40-0
tert-butyl (2S,5S)-6-amino-2-benzyloxycarbonylamino-5-[(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyloxy)-(1->2)-(3,4,6-tri-O-benzyl-β-D-galactopyranosyloxy)]hexanoate

: 220243-87-8
(S)-6-bromo-2-tert-butoxycarbonylamino-5-oxohexanoic acid tert-butyl ester

: 862674-27-9
C₁₀₉H₁₃₆N₄O₂₄

Guidance literature:: tert-butyl (2S,5S)-6-amino-2-benzyloxycarbonylamino-5-[(2,3,4,6-tetra-O-benzyl-α-D-glucopyranosyloxy)-(1->2)-(3,4,6-tri-O-benzyl-β-D-galactopyranosyloxy)]hexanoate; (S)-6-bromo-2-tert-butoxycarbonylamino-5-oxohexanoic acid tert-butyl ester; With sodium carbonate; In acetonitrile; at 20 ℃; for 8h;

With oxygen; In methanol; at 20 ℃; for 72h; Further stages.;
DOI:10.1016/j.tetasy.2007.10.037