bis(methyl4,6-O-benzylidene-2,3-dideoxy-α-D-glucopyranosido<2,3-b><2',3'-k>-1,4,7,10,13,16-hexaoxacyclo-octadecane

Base Information

• Chemical Name: bis(methyl4,6-O-benzylidene-2,3-dideoxy-α-D-glucopyranosido<2,3-b><2',3'-k>-1,4,7,10,13,16-hexaoxacyclo-octadecane
• CAS No.: 88269-03-8
• Molecular Formula: C₃₆H₄₈O₁₄
• Molecular Weight: 704.769

Synonyms:bis(methyl4,6-O-benzylidene-2,3-dideoxy-α-D-glucopyranosido<2,3-b><2',3'-k>-1,4,7,10,13,16-hexaoxacyclo-octadecane

Chemical Property of bis(methyl4,6-O-benzylidene-2,3-dideoxy-α-D-glucopyranosido<2,3-b><2',3'-k>-1,4,7,10,13,16-hexaoxacyclo-octadecane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of bis(methyl4,6-O-benzylidene-2,3-dideoxy-α-D-glucopyranosido<2,3-b><2',3'-k>-1,4,7,10,13,16-hexaoxacyclo-octadecane

There total 4 articles about bis(methyl4,6-O-benzylidene-2,3-dideoxy-α-D-glucopyranosido<2,3-b><2',3'-k>-1,4,7,10,13,16-hexaoxacyclo-octadecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

methyl 4,6-O-benzylidene-α-D-glucopyranoside (3162-96-7) + methyl 4,6-O-benzylidene-2,3-O--α-D-glucopyranoside → C36H48O14 (67077-31-0,67113-28-4,67113-30-8,85718-36-1,85718-38-3,85718-40-7) + bis(methyl4,6-O-benzylidene-2,3-dideoxy-α-D-glucopyranosido<2,3-b><2',3'-k>-1,4,7,10,13,16-hexaoxacyclo-octadecane (88269-03-8)

Guidance literature:

With tetra(n-butyl)ammonium hydroxide; In toluene; at 85 ℃; for 96h;

Reference yield: 12.0%

diethylene glycol ditosylate (7460-82-4) + methyl 4,6-O-benzylidene-α-D-galactopyranoside (64552-06-3) → (+)-Bis(methyl-4,6-O-benzyliden-2,3-didesoxy-α-D-galactopyranosido)<2,3-b:3',2'-k>-1,4,7,10,13,16-hexaoxacyclooctadecan (67077-31-0,67113-28-4,67113-30-8,85718-36-1,85718-38-3,85718-40-7) + (+)-Bis(methyl-4,6-O-benzyliden-2,3-didesoxy-α-D-galactopyranosido)<3,2-b:3',2'-k>-1,4,7,10,13,16-hexaoxacyclooctadecan (67077-32-1,67113-29-5,67113-31-9,85718-37-2,85718-39-4,88269-03-8,104154-38-3)

Guidance literature:

With potassium hydroxide; In dimethyl sulfoxide; at 50 ℃; for 48h;

Reference yield: 4.0%

diethylene glycol ditosylate (7460-82-4) + methyl-4,6-O-phenylmethylene-α-D-mannopyranoside (3162-96-7,4148-58-7,4153-17-7,4288-93-1,5328-47-2,6988-39-2,13566-32-0,14155-23-8,27994-50-9,37093-57-5,37093-59-7,57701-27-6,59168-66-0,64552-06-3,65391-13-1,65391-14-2,65530-26-9,66512-65-0,71117-36-7,71117-37-8,71117-41-4,72904-85-9,74560-56-8,79549-74-9,86783-81-5,96093-51-5,98633-13-7,110415-35-5,110415-36-6,110850-29-8,124020-29-7,126924-12-7,129263-21-4,131433-03-9,145920-49-6,146863-04-9) → (+)-Bis(methyl-4,6-O-benzyliden-2,3-didesoxy-α-D-mannopyranosido)<2,3-b:3',2'-k>-1,4,7,10,13,16-hexaoxacyclooctadecan (67077-31-0,67113-28-4,67113-30-8,85718-36-1,85718-38-3,85718-40-7) + (+)-Bis(methyl-4,6-O-benzyliden-2,3-didesoxy-α-D-mannopyranosido)<3,2-b:3',2'-k>-1,4,7,10,13,16-hexaoxacyclooctadecan (67077-32-1,67113-29-5,67113-31-9,85718-37-2,85718-39-4,88269-03-8,104154-38-3)

Guidance literature:

With sodium hydride; In dimethyl sulfoxide; at 50 ℃; for 120h;

upstream raw materials:

diethylene glycol ditosylate

4,6-O-benzylidene-1-O-methyl-α-D-glucopyranoside

methyl 4,6-O-benzylidene-α-D-glucopyranoside

methyl-4,6-O-phenylmethylene-α-D-mannopyranoside

Downstream raw materials:

bis(methyl 4-O-acetyl-2,3-dideoxy-6-O-trityl-α-D-glucopyranosido<2,3-b><2',3'-k>)-1,4,7,10,13,16-hexaoxacyclo-octadecane

bis(methyl 4-O-benzoyl-6-bromo-2,3-6-trideoxy-α-D-glucopyranosido<2,3-b><2',3'-k>)-1,4,7,10,13,16-hexaoxacyclo-octadecane

bis(methyl 4-O-benzyl-2,3-dideoxy-α-D-glucopyranosido<2,3-b><2',3'-k>)-1,4,7,10,13,16-hexaoxacyclo-octadecane

(methyl 4-O-benzyl-2,3-dideoxy-α-D-glucopyranosido<2,3-b>)-(methyl 6-O-benzyl-2,3-dideoxy-α-D-glucopyranosido<2',3'-k>)-1,4,7,10,13,16-hexaoxacyclo-octadecane

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