Technology Process of C37H43N3O7S2
There total 12 articles about C37H43N3O7S2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: toluene-4-sulfonic acid / 20 °C / Inert atmosphere
2: pyridine; triethylamine / dichloromethane / 20 °C / Inert atmosphere
3: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 20 °C / Inert atmosphere
With
pyridine; di-isopropyl azodicarboxylate; toluene-4-sulfonic acid; triethylamine; triphenylphosphine;
In
tetrahydrofuran; dichloromethane;
DOI:10.1021/jm2007062
- Guidance literature:
-
With
di-isopropyl azodicarboxylate; triphenylphosphine;
In
tetrahydrofuran;
at 20 ℃;
Inert atmosphere;
DOI:10.1021/jm2007062
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate / methanol / 1 h / 20 °C / Inert atmosphere
2: copper(l) iodide; bis(benzonitrile)palladium(II) chloride; tri-tert-butyl phosphine; diisopropylamine / 1,4-dioxane; hexane / 70 °C / Inert atmosphere
3: platinum(IV) oxide; hydrogen / ethanol; ethyl acetate / 20 °C / Inert atmosphere
4: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 20 °C / Inert atmosphere
With
platinum(IV) oxide; copper(l) iodide; bis(benzonitrile)palladium(II) chloride; tri-tert-butyl phosphine; di-isopropyl azodicarboxylate; hydrogen; potassium carbonate; diisopropylamine; triphenylphosphine;
In
tetrahydrofuran; 1,4-dioxane; methanol; ethanol; hexane; ethyl acetate;
DOI:10.1021/jm2007062