(E)-N-benzyl-N-[2-(3,4-dimethoxyphenyl)hexa-1,5-dienyl]-2-ethylsulfinylacetamide

Base Information

• Chemical Name: (E)-N-benzyl-N-[2-(3,4-dimethoxyphenyl)hexa-1,5-dienyl]-2-ethylsulfinylacetamide
• CAS No.: 499992-99-3
• Molecular Formula: C₂₅H₃₁NO₄S
• Molecular Weight: 441.591

Synonyms:(E)-N-benzyl-N-[2-(3,4-dimethoxyphenyl)hexa-1,5-dienyl]-2-ethylsulfinylacetamide

Chemical Property of (E)-N-benzyl-N-[2-(3,4-dimethoxyphenyl)hexa-1,5-dienyl]-2-ethylsulfinylacetamide

Chemical Property:

Purity/Quality:

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Technology Process of (E)-N-benzyl-N-[2-(3,4-dimethoxyphenyl)hexa-1,5-dienyl]-2-ethylsulfinylacetamide

There total 5 articles about (E)-N-benzyl-N-[2-(3,4-dimethoxyphenyl)hexa-1,5-dienyl]-2-ethylsulfinylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

(E)-N-benzyl-N-[2-(3,4-dimethoxyphenyl)hexa-1,5-dienyl]-2-ethylsulfanylacetamide (499993-26-9) → (E)-N-benzyl-N-[2-(3,4-dimethoxyphenyl)hexa-1,5-dienyl]-2-ethylsulfinylacetamide (499992-99-3)

Guidance literature:

With sodium periodate; In methanol; water; at 25 ℃; for 2.5h;

DOI:10.1021/jo026471g

Reference yield:

benzylamine (100-46-9) → (E)-N-benzyl-N-[2-(3,4-dimethoxyphenyl)hexa-1,5-dienyl]-2-ethylsulfinylacetamide (499992-99-3)

Guidance literature:

Multi-step reaction with 3 steps

1: benzene / 16 h / Heating

2: pyridine / CH₂Cl₂ / 2 h / 25 °C

3: 60 percent / sodium periodate / H₂O; methanol / 2.5 h / 25 °C

With pyridine; sodium periodate; In methanol; dichloromethane; water; benzene;

DOI:10.1021/jo026471g

Reference yield:

2-(3,4-dimethoxyphenyl)hex-5-enal (499993-23-6) → (E)-N-benzyl-N-[2-(3,4-dimethoxyphenyl)hexa-1,5-dienyl]-2-ethylsulfinylacetamide (499992-99-3)

Guidance literature:

Multi-step reaction with 3 steps

1: benzene / 16 h / Heating

2: pyridine / CH₂Cl₂ / 2 h / 25 °C

3: 60 percent / sodium periodate / H₂O; methanol / 2.5 h / 25 °C

With pyridine; sodium periodate; In methanol; dichloromethane; water; benzene;

DOI:10.1021/jo026471g

upstream raw materials:

(E)-N-benzyl-N-[2-(3,4-dimethoxyphenyl)hexa-1,5-dienyl]-2-ethylsulfanylacetamide

benzylamine

2-(3,4-dimethoxyphenyl)hex-5-enal

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