((1S,2R,3S,4S,5S,6R)-2,3,4-Tris-benzyloxy-5,6-dihydroxy-cyclohexyl)-acetic acid

Base Information

Chemical Name:((1S,2R,3S,4S,5S,6R)-2,3,4-Tris-benzyloxy-5,6-dihydroxy-cyclohexyl)-acetic acid
CAS No.:215303-33-6
Molecular Formula:C₂₉H₃₂O₇
Molecular Weight:492.569
Hs Code.:

Synonyms:((1S,2R,3S,4S,5S,6R)-2,3,4-Tris-benzyloxy-5,6-dihydroxy-cyclohexyl)-acetic acid

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Chemical Property of ((1S,2R,3S,4S,5S,6R)-2,3,4-Tris-benzyloxy-5,6-dihydroxy-cyclohexyl)-acetic acid

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Technology Process of ((1S,2R,3S,4S,5S,6R)-2,3,4-Tris-benzyloxy-5,6-dihydroxy-cyclohexyl)-acetic acid

There total 1 articles about ((1S,2R,3S,4S,5S,6R)-2,3,4-Tris-benzyloxy-5,6-dihydroxy-cyclohexyl)-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 215303-30-3
((1S,2R,3R,4S,5R,6S)-3,4,5-Tris-benzyloxy-7-oxa-bicyclo[4.1.0]hept-2-yl)-acetic acid methyl ester

: 215303-33-6
((1S,2R,3S,4S,5S,6R)-2,3,4-Tris-benzyloxy-5,6-dihydroxy-cyclohexyl)-acetic acid

Guidance literature:: With potassium carbonate; In methanol; water; for 20h; Ambient temperature;
DOI:10.1021/jo981211d

Reference yield: 52.0%

: 215303-33-6
((1S,2R,3S,4S,5S,6R)-2,3,4-Tris-benzyloxy-5,6-dihydroxy-cyclohexyl)-acetic acid

: (3aR,4R,5S,6S,7S,7aR)-4,5,6-Tris-benzyloxy-7-hydroxy-hexahydro-benzofuran-2-one

Guidance literature:: With 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; for 1h;
DOI:10.1021/jo981211d

Reference yield:

: 215303-33-6
((1S,2R,3S,4S,5S,6R)-2,3,4-Tris-benzyloxy-5,6-dihydroxy-cyclohexyl)-acetic acid

: ((1R,2R,3S,4R,5S,6R)-2,3-Diacetoxy-4,5,6-tris-benzyloxy-cyclohexyl)-acetic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: diethyl ether

2: pyridine, DMAP / CH₂Cl₂ / 1 h / Ambient temperature

With pyridine; dmap; In diethyl ether; dichloromethane;
DOI:10.1021/jo981211d