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4-BrC6H4SbI2

Base Information
  • Chemical Name:4-BrC6H4SbI2
  • CAS No.:856161-89-2
  • Molecular Formula:C6H4BrI2Sb
  • Molecular Weight:531.561
  • Hs Code.:
4-BrC<sub>6</sub>H<sub>4</sub>SbI<sub>2</sub>

Synonyms:4-BrC6H4SbI2

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Chemical Property of 4-BrC6H4SbI2
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Technology Process of 4-BrC6H4SbI2

There total 2 articles about 4-BrC6H4SbI2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With ammonia; hydrogen iodide; In acetic acid; acetone; with aq. NH3 at 0°C then 4-BrC6H4SbO is isolated, dissolved in acetic acid; pptn. with HI;
DOI:10.1021/ja01330a056
Guidance literature:
With potassium iodide; tin(ll) chloride; In hydrogenchloride; water; reduction with SnCl2 then treated the soln. with satd. aq. KI soln.;
Guidance literature:
With magnesium; In diethyl ether; benzene; C6H5SbI2 in benzene slowly added to the Grignard reagent of 2,2'-dibromo-4-methyldiphenylether in ether; distn. the ether, cooled the benzene soln., treated with ice and HCl, distn. the benzene layer; product was chlorinated in CCl4 and reduced by passing H2S in hot ethanol/ammonia, placed in ice to form feathery needles;
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