Phenyl 3-O-2-propen-1-yl-1-thio-beta-D-galactopyranoside

Base Information

Chemical Name:Phenyl 3-O-2-propen-1-yl-1-thio-beta-D-galactopyranoside
CAS No.:400091-17-0
Molecular Formula:C₁₅H₂₀O₅S
Molecular Weight:312.387
Hs Code.:
DSSTox Substance ID:DTXSID301215148

Synonyms:DTXSID301215148;Phenyl 3-O-2-propen-1-yl-1-thio-beta-D-galactopyranoside;400091-17-0

Suppliers and Price of Phenyl 3-O-2-propen-1-yl-1-thio-beta-D-galactopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of Phenyl 3-O-2-propen-1-yl-1-thio-beta-D-galactopyranoside

Chemical Property:

XLogP3:1.5
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:6
Exact Mass:312.10314491
Heavy Atom Count:21
Complexity:321

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C=CCOC1C(C(OC(C1O)SC2=CC=CC=C2)CO)O
Isomeric SMILES:C=CCO[C@H]1[C@H]([C@H](O[C@H]([C@@H]1O)SC2=CC=CC=C2)CO)O

Technology Process of Phenyl 3-O-2-propen-1-yl-1-thio-beta-D-galactopyranoside

There total 2 articles about Phenyl 3-O-2-propen-1-yl-1-thio-beta-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 16758-34-2
1-thiophenyl-β-D-galactopyranoside

: 106-95-6
allyl bromide

: 400091-17-0
phenyl 3-O-allyl-1-thio-β-D-galactopyranoside

Guidance literature:: 1-thiophenyl-β-D-galactopyranoside; With di(n-butyl)tin oxide; In methanol; for 3h; Heating;

allyl bromide; With tetra-(n-butyl)ammonium iodide; In 1,4-dioxane; Heating;
DOI:10.1515/znb-2003-0808

Reference yield:

: 13992-16-0,23661-28-1,28512-68-7,65236-85-3,86782-39-0,108032-93-5,121524-01-4,121570-34-1,24404-53-3
1-deoxy-1-(phenylthio)-2,3,4,6-tetra-O-acetyl-β-D-galactopyranose

: 400091-17-0
phenyl 3-O-allyl-1-thio-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: 77 percent / NaOMe / methanol / 4 h / 20 °C

2.1: Bu₂SnO / methanol / 3 h / Heating

2.2: 87 percent / Bu₄NI / dioxane / Heating

With sodium methylate; di(n-butyl)tin oxide; In methanol;
DOI:10.1515/znb-2003-0808

Reference yield: 94.0%

: 1125-88-8
benzaldehyde dimethyl acetal

: 400091-17-0
phenyl 3-O-allyl-1-thio-β-D-galactopyranoside

: 400091-18-1
phenyl 3-O-allyl-4,6-O-benzylidene-1-thio-β-D-galactopyranoside

Guidance literature:: With toluene-4-sulfonic acid; In tetrahydrofuran; at 25 ℃; for 2h;
DOI:10.1002/1099-0690(200110)2001:20<3849::AID-EJOC3849>3.0.CO;2-Q