N-[[2'-[2-(triphenylmethyl)-2H-tetrazol-5-yl][1,1'-biphenyl]-4-yl]methyl]-L-valine 1,1-dimethylethyl ester

Base Information

• Chemical Name: N-[[2'-[2-(triphenylmethyl)-2H-tetrazol-5-yl][1,1'-biphenyl]-4-yl]methyl]-L-valine 1,1-dimethylethyl ester
• CAS No.: 924654-09-1
• Molecular Formula: C₄₂H₄₃N₅O₂
• Molecular Weight: 649.836

Synonyms:N-[[2'-[2-(triphenylmethyl)-2H-tetrazol-5-yl][1,1'-biphenyl]-4-yl]methyl]-L-valine 1,1-dimethylethyl ester

Chemical Property of N-[[2'-[2-(triphenylmethyl)-2H-tetrazol-5-yl][1,1'-biphenyl]-4-yl]methyl]-L-valine 1,1-dimethylethyl ester

Chemical Property:

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Technology Process of N-[[2'-[2-(triphenylmethyl)-2H-tetrazol-5-yl][1,1'-biphenyl]-4-yl]methyl]-L-valine 1,1-dimethylethyl ester

There total 1 articles about N-[[2'-[2-(triphenylmethyl)-2H-tetrazol-5-yl][1,1'-biphenyl]-4-yl]methyl]-L-valine 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

(E) N-[[2'-[2-(triphenylmethyl)-2H-tetrazol-5-yl][1,1'-biphenyl]-4-yl]methylene]-L-valine 1,1-dimethylethyl ester (924654-07-9) → N-[[2'-[2-(triphenylmethyl)-2H-tetrazol-5-yl][1,1'-biphenyl]-4-yl]methyl]-L-valine 1,1-dimethylethyl ester (924654-09-1)

Guidance literature:

With sodium cyanoborohydride; In tetrahydrofuran; methanol; at 0 - 20 ℃; for 20h;

Reference yield: 42.0%

6-(nitrooxy)hexanoyl chloride (907625-06-3) + N-[[2'-[2-(triphenylmethyl)-2H-tetrazol-5-yl][1,1'-biphenyl]-4-yl]methyl]-L-valine 1,1-dimethylethyl ester (924654-09-1) → N-[6-(nitrooxy)-1-oxohexyl]-N-[[2'-[2-(triphenylmethyl)-2H-tetrazol-5-yl][1,1'-biphenyl]-4-yl]methyl]-L-valine 1,1-dimethylethyl ester (924654-11-5)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 21h;

Reference yield: 10.0%

5,6-bis(nitrooxy)hexanoic acid (849113-53-7) + N-[[2'-[2-(triphenylmethyl)-2H-tetrazol-5-yl][1,1'-biphenyl]-4-yl]methyl]-L-valine 1,1-dimethylethyl ester (924654-09-1) → N-[5,6-bis(nitrooxy)-1-oxohexyl]-N-[[2'-[2-(triphenylmethyl)-2H-tetrazol-5-yl][1,1'-biphenyl]-4-yl]methyl]-L-valine 1,1-dimethylethyl ester (924654-17-1)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃;

upstream raw materials:

(E) N-[[2'-[2-(triphenylmethyl)-2H-tetrazol-5-yl][1,1'-biphenyl]-4-yl]methylene]-L-valine 1,1-dimethylethyl ester

Downstream raw materials:

N-[5,6-bis(nitrooxy)-1-oxohexyl]-N-[[2'-[2-(triphenylmethyl)-2H-tetrazol-5-yl][1,1'-biphenyl]-4-yl]methyl]-L-valine 1,1-dimethylethyl ester

N-[3-[(nitrooxy)methyl]benzoyl]-N-[[2'-[2-(triphenylmethyl)-2H-tetrazol-5-yl][1,1'-biphenyl]-4-yl]methyl]-L-valine 1,1-dimethylethyl ester

N-[6-(nitrooxy)-1-oxohexyl]-N-[[2'-[2-(triphenylmethyl)-2H-tetrazol-5-yl][1,1'-biphenyl]-4-yl]methyl]-L-valine 1,1-dimethylethyl ester

N-[4,5-bis(nitrooxy)-1-oxopentyl]-N-[[2'-[2-(triphenylmethyl)-2H-tetrazol-5-yl][1,1'-biphenyl]-4-yl]methyl]-L-valine 1,1-dimethylethyl ester

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