N-(3-(2-hydroxy-6-(3-hydroxyphenyl)naphthalen-1-yl)phenyl)quinolin-6-sulfonamide

Base Information

Chemical Name:N-(3-(2-hydroxy-6-(3-hydroxyphenyl)naphthalen-1-yl)phenyl)quinolin-6-sulfonamide
CAS No.:1365957-78-3
Molecular Formula:C₃₁H₂₂N₂O₄S
Molecular Weight:518.593
Hs Code.:

Synonyms:N-(3-(2-hydroxy-6-(3-hydroxyphenyl)naphthalen-1-yl)phenyl)quinolin-6-sulfonamide

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Chemical Property of N-(3-(2-hydroxy-6-(3-hydroxyphenyl)naphthalen-1-yl)phenyl)quinolin-6-sulfonamide

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Technology Process of N-(3-(2-hydroxy-6-(3-hydroxyphenyl)naphthalen-1-yl)phenyl)quinolin-6-sulfonamide

There total 6 articles about N-(3-(2-hydroxy-6-(3-hydroxyphenyl)naphthalen-1-yl)phenyl)quinolin-6-sulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1365958-48-0
N-(3-(2-methoxy-6-(3-methoxyphenyl)naphthalen-1-yl)phenyl)quinoline-6-sulfonamide

: 1365957-78-3
N-(3-(2-hydroxy-6-(3-hydroxyphenyl)naphthalen-1-yl)phenyl)quinolin-6-sulfonamide

Guidance literature:: With boron tribromide; In dichloromethane; at -25 - 20 ℃; for 4h;
DOI:10.1021/jm201735j

Reference yield:

: 65433-99-0
quinoline-6-sulfonyl chloride

: 1064680-92-7
1-(3-aminophenyl)-6-(3-hydroxyphenyl)naphthalen-2-ol

: 1365957-78-3
N-(3-(2-hydroxy-6-(3-hydroxyphenyl)naphthalen-1-yl)phenyl)quinolin-6-sulfonamide

Guidance literature:: quinoline-6-sulfonyl chloride; 1-(3-aminophenyl)-6-(3-hydroxyphenyl)naphthalen-2-ol; With polystyrene supported morpholine; In tetrahydrofuran; at 20 ℃; for 15h;

With polystyrene supported dimethylaminopyridine; In tetrahydrofuran; at 60 ℃; for 15h;
DOI:10.1021/jm201735j

Reference yield:

: 1041115-67-6
1-bromo-2-methoxy-6-(3-methoxyphenyl)naphthalene

: 1365957-78-3
N-(3-(2-hydroxy-6-(3-hydroxyphenyl)naphthalen-1-yl)phenyl)quinolin-6-sulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; caesium carbonate / 1,2-dimethoxyethane; ethanol; water / 0.25 h / 150 °C / 1125.11 Torr / Microwave irradiation

2.1: boron tribromide / dichloromethane / 18 h / -78 - 20 °C

3.1: polystyrene supported morpholine / tetrahydrofuran / 15 h / 20 °C

3.2: polystyrene supported dimethylaminopyridine / 15 h / 60 °C

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; boron tribromide; caesium carbonate; In tetrahydrofuran; 1,2-dimethoxyethane; ethanol; dichloromethane; water; 1.1: Suzuki coupling;
DOI:10.1021/jm201735j