[Pd(2-((dimethylamino)methyl)phenyl-C⁽¹⁾,N)(PPh₃)[N_.tplbond.C-C(H)=PPh₃]](ClO₄)

Base Information

• Chemical Name: [Pd(2-((dimethylamino)methyl)phenyl-C⁽¹⁾,N)(PPh₃)[N_.tplbond.C-C(H)=PPh₃]](ClO₄)
• CAS No.: 187245-92-7
• Molecular Formula: C₄₇H₄₃N₂P₂Pd*ClO₄
• Molecular Weight: 903.69

Synonyms:[Pd(2-((dimethylamino)methyl)phenyl-C⁽¹⁾,N)(PPh₃)[N_.tplbond.C-C(H)=PPh₃]](ClO₄)

Chemical Property of [Pd(2-((dimethylamino)methyl)phenyl-C⁽¹⁾,N)(PPh₃)[N_.tplbond.C-C(H)=PPh₃]](ClO₄)

Chemical Property:

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Technology Process of [Pd(2-((dimethylamino)methyl)phenyl-C⁽¹⁾,N)(PPh₃)[N_.tplbond.C-C(H)=PPh₃]](ClO₄)

There total 5 articles about [Pd(2-((dimethylamino)methyl)phenyl-C⁽¹⁾,N)(PPh₃)[N_.tplbond.C-C(H)=PPh₃]](ClO₄) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

μ-chloro-([2-(N,N-dimethylamino)methyl]phenyl-C,N)(triphenylphosphine-P)palladium(II) + silver perchlorate + cyanomethylene triphenylphosphorane (16640-68-9) → [Pd(2-((dimethylamino)methyl)phenyl-C(1),N)(PPh3)[N.tplbond.C-C(H)=PPh3]](ClO4) (187245-92-7)

Guidance literature:

With THF; In tetrahydrofuran; byproducts: AgCl; stirring Pd-complex with 1 equiv. AgClO4 for 30 min (room temp., in dark), filtration off of AgCl, addn. of 1 equiv. ylide at 0°C, stirring at 0°C for 30 min; evapn., treatment with Et2O, collection (filtration), drying in air;

DOI:10.1021/ic960904e

Reference yield:

cyanomethylene triphenylphosphorane (16640-68-9) → [Pd(2-((dimethylamino)methyl)phenyl-C(1),N)(PPh3)[N.tplbond.C-C(H)=PPh3]](ClO4) (187245-92-7)

Guidance literature:

Multi-step reaction with 3 steps

1: dichloromethane

2: dichloromethane

3: chloroform-d1

In chloroform-d1; dichloromethane;

DOI:10.1021/ic960904e

Reference yield:

bis(acetonitrile-κN)([(2-dimethylamino-κN)methyl]phenyl-κC(1))palladium(II) perchlorate → [Pd(2-((dimethylamino)methyl)phenyl-C(1),N)(PPh3)[N.tplbond.C-C(H)=PPh3]](ClO4) (187245-92-7)

Guidance literature:

Multi-step reaction with 3 steps

1: dichloromethane

2: dichloromethane

3: chloroform-d1

In chloroform-d1; dichloromethane;

DOI:10.1021/ic960904e

upstream raw materials:

cyanomethylene triphenylphosphorane

[Pd(2-((dimethylamino)methyl)phenyl-C⁽¹⁾,N)[C(H)(C_.tplbond.N)(PPh₃)][N_.tplbond.C-C(H)=PPh₃]](ClO₄)

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