(R_S,R)-N-(3-hydroxy-5-methyl-1-phenylhexylidene)-tert-butanesulfonamide

Base Information

• Chemical Name: (R_S,R)-N-(3-hydroxy-5-methyl-1-phenylhexylidene)-tert-butanesulfonamide
• CAS No.: 441788-42-7
• Molecular Formula: C₁₇H₂₇NO₂S
• Molecular Weight: 309.473

Synonyms:(R_S,R)-N-(3-hydroxy-5-methyl-1-phenylhexylidene)-tert-butanesulfonamide

Chemical Property of (R_S,R)-N-(3-hydroxy-5-methyl-1-phenylhexylidene)-tert-butanesulfonamide

Chemical Property:

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Technology Process of (R_S,R)-N-(3-hydroxy-5-methyl-1-phenylhexylidene)-tert-butanesulfonamide

There total 1 articles about (R_S,R)-N-(3-hydroxy-5-methyl-1-phenylhexylidene)-tert-butanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

isovaleraldehyde (590-86-3) + (E)-(±)-N-α-methyl(phenylmethylidene)-tert-butanesulfinamide (729559-17-5) → (RS,R)-N-(3-hydroxy-5-methyl-1-phenylhexylidene)-tert-butanesulfonamide (441788-42-7) + (RS,S)-N-(3-hydroxy-5-methyl-1-phenylhexylidene)-tert-butanesulfinamide

Guidance literature:

(E)-(±)-N-α-methyl(phenylmethylidene)-tert-butanesulfinamide; With lithium diisopropyl amide; In tetrahydrofuran; at -78 ℃; for 0.75h;

With magnesium bromide; In tetrahydrofuran; at -78 ℃; for 0.75h;

isovaleraldehyde; In tetrahydrofuran; at -78 ℃; for 3h;

DOI:10.1021/ja026292g

Reference yield: 84.0%

(RS,R)-N-(3-hydroxy-5-methyl-1-phenylhexylidene)-tert-butanesulfonamide (441788-42-7) → (RS,1R,3R)-2-methylpropane-2-sulfinic acid (3-hydroxy-5-methyl-1-phenyl-hexyl)amide + (RS,1S,3R)-2-methylpropane-2-sulfinic acid (3-hydroxy-5-methyl-1-phenyl-hexyl)amide

Guidance literature:

With benzo[1,3,2]dioxaborole; In tetrahydrofuran; at -10 ℃; for 20h;

DOI:10.1021/ja026292g

Reference yield: 83.0%

(RS,R)-N-(3-hydroxy-5-methyl-1-phenylhexylidene)-tert-butanesulfonamide (441788-42-7) → (RS,1S,3R)-2-methylpropane-2-sulfinic acid (3-hydroxy-5-methyl-1-phenyl-hexyl)amide

Guidance literature:

With lithium triethylborohydride; In tetrahydrofuran; at -78 ℃; for 3h;

DOI:10.1021/ja026292g DOI:10.1021/ja0363462

upstream raw materials:

isovaleraldehyde

(E)-(±)-N-α-methyl(phenylmethylidene)-tert-butanesulfinamide

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