2-nitro-N-hexadecylbenzenesulfonamide

Base Information

• Chemical Name: 2-nitro-N-hexadecylbenzenesulfonamide
• CAS No.: 198971-44-7
• Molecular Formula: C₂₂H₃₈N₂O₄S
• Molecular Weight: 426.621
• Mol file: 198971-44-7.mol

Synonyms:2-nitro-N-hexadecylbenzenesulfonamide

Chemical Property of 2-nitro-N-hexadecylbenzenesulfonamide

Chemical Property:

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Technology Process of 2-nitro-N-hexadecylbenzenesulfonamide

There total 1 articles about 2-nitro-N-hexadecylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

hexadecylamine (143-27-1) + 2-Nitrobenzenesulfonyl chloride (1694-92-4) → 2-nitro-N-hexadecylbenzenesulfonamide (198971-44-7)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 23 ℃; for 1.25h; Large scale reaction;

DOI:10.1039/b814598a

Reference yield: 99.0%

2-nitro-N-hexadecylbenzenesulfonamide (198971-44-7) + 2-(2-(2-methoxyethoxy)ethoxy)ethyl p-toluenesulfonate (62921-74-8,518012-62-9,58320-73-3) → N-(3,6,9-trioxadecyl)-2-nitro-N-octylbenzenesulfonamide

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 60 ℃; for 16h; Inert atmosphere;

DOI:10.1039/b814598a

upstream raw materials:

hexadecylamine

2-Nitrobenzenesulfonyl chloride