(E,Z)-5-<(4-Methoxyphenyl)methoxy>-3-<<(4-methoxyphenyl)methoxy>methyl>-2-<2-<<2-(trimethylsilyl)ethoxy>methoxy>ethylidene>-3-pentenoic acid methyl ester

Base Information

Chemical Name:(E,Z)-5-<(4-Methoxyphenyl)methoxy>-3-<<(4-methoxyphenyl)methoxy>methyl>-2-<2-<<2-(trimethylsilyl)ethoxy>methoxy>ethylidene>-3-pentenoic acid methyl ester
CAS No.:167964-25-2
Molecular Formula:C₃₁H₄₄O₈Si
Molecular Weight:572.771
Hs Code.:

(E,Z)-5-<(4-Methoxyphenyl)methoxy>-3-<<(4-methoxyphenyl)methoxy>methyl>-2-<2-<<2-(trimethylsilyl)ethoxy>methoxy>ethylidene>-3-pentenoic acid methyl ester

Synonyms:(E,Z)-5-<(4-Methoxyphenyl)methoxy>-3-<<(4-methoxyphenyl)methoxy>methyl>-2-<2-<<2-(trimethylsilyl)ethoxy>methoxy>ethylidene>-3-pentenoic acid methyl ester

Suppliers and Price of (E,Z)-5-<(4-Methoxyphenyl)methoxy>-3-<<(4-methoxyphenyl)methoxy>methyl>-2-<2-<<2-(trimethylsilyl)ethoxy>methoxy>ethylidene>-3-pentenoic acid methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of (E,Z)-5-<(4-Methoxyphenyl)methoxy>-3-<<(4-methoxyphenyl)methoxy>methyl>-2-<2-<<2-(trimethylsilyl)ethoxy>methoxy>ethylidene>-3-pentenoic acid methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (E,Z)-5-<(4-Methoxyphenyl)methoxy>-3-<<(4-methoxyphenyl)methoxy>methyl>-2-<2-<<2-(trimethylsilyl)ethoxy>methoxy>ethylidene>-3-pentenoic acid methyl ester

There total 4 articles about (E,Z)-5-<(4-Methoxyphenyl)methoxy>-3-<<(4-methoxyphenyl)methoxy>methyl>-2-<2-<<2-(trimethylsilyl)ethoxy>methoxy>ethylidene>-3-pentenoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: (E/Z)-2-Iodo-4-<<2-(trimethylsilyl)ethoxy>methoxy>-2-butenoic acid methyl ester

: Tributyl-[(E)-3-(4-methoxy-benzyloxy)-1-(4-methoxy-benzyloxymethyl)-propenyl]-stannane

: 167964-25-2
(E,Z)-5-<(4-Methoxyphenyl)methoxy>-3-<<(4-methoxyphenyl)methoxy>methyl>-2-<2-<<2-(trimethylsilyl)ethoxy>methoxy>ethylidene>-3-pentenoic acid methyl ester

Guidance literature:: With dichloro bis(acetonitrile) palladium(II); In N,N-dimethyl-formamide; at 25 ℃; for 72h;

Reference yield:

: 824-94-2
p-methoxybenzyl chloride

: 167964-25-2
(E,Z)-5-<(4-Methoxyphenyl)methoxy>-3-<<(4-methoxyphenyl)methoxy>methyl>-2-<2-<<2-(trimethylsilyl)ethoxy>methoxy>ethylidene>-3-pentenoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / NaH, n-Bu₄NI / tetrahydrofuran / 1.) 22 deg C, 2.) 22 deg C, 12 h

2: 1.) n-Bu₃SnH / 1.) Pd(Ph₃P)2Cl₂, 2.) Pd(CH₃CN)2Cl₂ / 1.) THF, 22 deg C, 17 h, 2.) DMF, 22 deg C, 3 d

With tri-n-butyl-tin hydride; tetra-(n-butyl)ammonium iodide; sodium hydride; bis-triphenylphosphine-palladium(II) chloride; dichloro bis(acetonitrile) palladium(II); In tetrahydrofuran;

Reference yield:

: 152857-09-5
1,4--2-butyne

: (E/Z)-2-Iodo-4-<<2-(trimethylsilyl)ethoxy>methoxy>-2-butenoic acid methyl ester

: 167964-25-2
(E,Z)-5-<(4-Methoxyphenyl)methoxy>-3-<<(4-methoxyphenyl)methoxy>methyl>-2-<2-<<2-(trimethylsilyl)ethoxy>methoxy>ethylidene>-3-pentenoic acid methyl ester

Guidance literature:: With tri-n-butyl-tin hydride; bis-triphenylphosphine-palladium(II) chloride; dichloro bis(acetonitrile) palladium(II); Yield given. Multistep reaction; 1.) THF, 22 deg C, 17 h, 2.) DMF, 22 deg C, 3 d;