AKOS BBS-00003291

Base Information

• Chemical Name: AKOS BBS-00003291
• CAS No.: 29527-31-9
• Molecular Formula: C₁₁H₁₃N₃S
• Molecular Weight: 219.31
• Mol file: 29527-31-9.mol

Synonyms:4-ethyl-5-(4-methylphenyl)-4H-1,2,4-triazole-3-thiol

Chemical Property of AKOS BBS-00003291

Chemical Property:

• Boiling Point: 301.8±35.0 °C(Predicted)
• PKA: 8.41±0.20(Predicted)
• Density: 1.21±0.1 g/cm3(Predicted)

Purity/Quality:

98%min ^*data from raw suppliers

4-ethyl-5-(4-methylphenyl)-4H-1,2,4-triazole-3-thiol ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi,Xn
• Statements: 22

MSDS Files:

Useful:

Technology Process of AKOS BBS-00003291

There total 3 articles about AKOS BBS-00003291 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.7%

C11H15N3OS (29527-13-7) → 4-ethyl-5-(4-methylphenyl)-4H-1,2,4-triazole-3-thiol (29527-31-9)

Guidance literature:

With sodium hydroxide; Reflux;

DOI:10.2174/1570180815666180810122226

Reference yield:

p-toluic hydrazide (3619-22-5) → 4-ethyl-5-(4-methylphenyl)-4H-1,2,4-triazole-3-thiol (29527-31-9)

Guidance literature:

Multi-step reaction with 2 steps

1: Reflux

2: sodium hydroxide / Reflux

With sodium hydroxide;

DOI:10.2174/1570180815666180810122226

Reference yield:

→ 4-ethyl-5-(4-methylphenyl)-4H-1,2,4-triazole-3-thiol (29527-31-9)

Guidance literature:

Thiosemicarbazid 5, NaOH;

DOI:10.1021/jm00298a021

upstream raw materials:

C₁₁H₁₅N₃OS

p-toluic hydrazide

Refernces

• 1、 -. "NEW COMPOUNDS". Page 143. . Retrieved 2010/02/06.